Análise por injeção em fluxo com detecção amperométrica de múltiplos pulsos: potencialidades e aplicações

The potentialities and applications of the Multiple Pulse Amperometric detection (MPA) coupled with Flow Injection Analysis (FIA) are evaluated. Important aspects as cleaning and activation of electrode surface, indirect and simultaneous analysis of electroactive compounds and the use of the interna...

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Veröffentlicht in:Química Nova 2011, Vol.34 (10), p.1753-1761
Hauptverfasser: Santos, Wallans Torres Pio dos, Gimenes, Denise Tofanello, Richter, Eduardo Mathias, Angnes, Lúcio
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container_title Química Nova
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creator Santos, Wallans Torres Pio dos
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description The potentialities and applications of the Multiple Pulse Amperometric detection (MPA) coupled with Flow Injection Analysis (FIA) are evaluated. Important aspects as cleaning and activation of electrode surface, indirect and simultaneous analysis of electroactive compounds and the use of the internal standard method for quantifications utilizing FIA-MPA are presented. The main parameters concerning the detection of electroactive analytes by multiple pulse amperometric detection in flowing solutions were also discussed. In addition, aspects such as flow rate, sample volume, application time of the potential pulses and instrumentation necessary for implementing of the method were also addressed.
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subjects electrochemical detection
flow injection analysis
multiple pulse amperometry
title Análise por injeção em fluxo com detecção amperométrica de múltiplos pulsos: potencialidades e aplicações
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