Análise por injeção em fluxo com detecção amperométrica de múltiplos pulsos: potencialidades e aplicações
The potentialities and applications of the Multiple Pulse Amperometric detection (MPA) coupled with Flow Injection Analysis (FIA) are evaluated. Important aspects as cleaning and activation of electrode surface, indirect and simultaneous analysis of electroactive compounds and the use of the interna...
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Veröffentlicht in: | Química Nova 2011, Vol.34 (10), p.1753-1761 |
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creator | Santos, Wallans Torres Pio dos Gimenes, Denise Tofanello Richter, Eduardo Mathias Angnes, Lúcio |
description | The potentialities and applications of the Multiple Pulse Amperometric detection (MPA) coupled with Flow Injection Analysis (FIA) are evaluated. Important aspects as cleaning and activation of electrode surface, indirect and simultaneous analysis of electroactive compounds and the use of the internal standard method for quantifications utilizing FIA-MPA are presented. The main parameters concerning the detection of electroactive analytes by multiple pulse amperometric detection in flowing solutions were also discussed. In addition, aspects such as flow rate, sample volume, application time of the potential pulses and instrumentation necessary for implementing of the method were also addressed. |
doi_str_mv | 10.1590/S0100-40422011001000008 |
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subjects | electrochemical detection flow injection analysis multiple pulse amperometry |
title | Análise por injeção em fluxo com detecção amperométrica de múltiplos pulsos: potencialidades e aplicações |
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