Crystal Structures and Properties of ZnO Nanopowders Prepared by Ultrasonic Method
Ultra-fine zinc oxide powders were prepared using ultrasonic method at 60°C with zinc acetate, zinc nitrate and potassium hydroxide solution as precursors. The obtained powders were characterized by means of scanning electron microscope, thermogravimetric analysis, X-ray diffraction and infrared spe...
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| Veröffentlicht in: | E-journal of surface science and nanotechnology 2011/12/27, Vol.9, pp.482-485 |
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| container_title | E-journal of surface science and nanotechnology |
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| creator | Anh, Dao Thi Ngoc Phuong, Huynh Thi Lan Thao, Hoang Thi Huong Ha, Nguyen Thi Cam Hoan, Nguyen Xuan |
| description | Ultra-fine zinc oxide powders were prepared using ultrasonic method at 60°C with zinc acetate, zinc nitrate and potassium hydroxide solution as precursors. The obtained powders were characterized by means of scanning electron microscope, thermogravimetric analysis, X-ray diffraction and infrared spectroscopy. The crystal structures were investigated based on Rietveld method. The results showed that, zinc oxide powders have hexagonal structure (P63mc) with particle size in the range of 100-300 nm. The mechanism for the ZnO formation was discussed. The properties of synthesized materials were examined by UV-Vis spectrum and cyclic voltammetry measurement. [DOI: 10.1380/ejssnt.2011.482] |
| doi_str_mv | 10.1380/ejssnt.2011.482 |
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The obtained powders were characterized by means of scanning electron microscope, thermogravimetric analysis, X-ray diffraction and infrared spectroscopy. The crystal structures were investigated based on Rietveld method. The results showed that, zinc oxide powders have hexagonal structure (P63mc) with particle size in the range of 100-300 nm. The mechanism for the ZnO formation was discussed. The properties of synthesized materials were examined by UV-Vis spectrum and cyclic voltammetry measurement. 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Surf. Sci. Nanotechnol.</addtitle><description>Ultra-fine zinc oxide powders were prepared using ultrasonic method at 60°C with zinc acetate, zinc nitrate and potassium hydroxide solution as precursors. The obtained powders were characterized by means of scanning electron microscope, thermogravimetric analysis, X-ray diffraction and infrared spectroscopy. The crystal structures were investigated based on Rietveld method. The results showed that, zinc oxide powders have hexagonal structure (P63mc) with particle size in the range of 100-300 nm. The mechanism for the ZnO formation was discussed. The properties of synthesized materials were examined by UV-Vis spectrum and cyclic voltammetry measurement. 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Surf. Sci. Nanotechnol.</addtitle><date>2011-01-01</date><risdate>2011</risdate><volume>9</volume><spage>482</spage><epage>485</epage><pages>482-485</pages><issn>1348-0391</issn><eissn>1348-0391</eissn><abstract>Ultra-fine zinc oxide powders were prepared using ultrasonic method at 60°C with zinc acetate, zinc nitrate and potassium hydroxide solution as precursors. The obtained powders were characterized by means of scanning electron microscope, thermogravimetric analysis, X-ray diffraction and infrared spectroscopy. The crystal structures were investigated based on Rietveld method. The results showed that, zinc oxide powders have hexagonal structure (P63mc) with particle size in the range of 100-300 nm. The mechanism for the ZnO formation was discussed. The properties of synthesized materials were examined by UV-Vis spectrum and cyclic voltammetry measurement. 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| subjects | Crystal structure Cyclic voltammetry Nanopowders Ultrasonic method Zinc oxide |
| title | Crystal Structures and Properties of ZnO Nanopowders Prepared by Ultrasonic Method |
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