Synthesis of Methyl 2, 3-, 2, 4- and 3, 4-Di-O-Methyl-α-D-Fucopyranosides
Methyl 2, 3-(15), 2, 4-(11) and 3, 4-di-O-methyl-α-D-fucopyranosides (8) were prepared from methyl α-D-fucopyranoside via methyl 3, 4-O-isopropylidene-α-D-fucopyranoside. These substances were required in connection with methylation analysis of saponins containing D-fucose residues. Compounds 8 and...
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Veröffentlicht in: | Chemical & pharmaceutical bulletin 1980/02/25, Vol.28(2), pp.632-634 |
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container_title | Chemical & pharmaceutical bulletin |
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creator | TAKEDA, TADAHIRO TAKABE, SEIICHI OGIHARA, YUKIO |
description | Methyl 2, 3-(15), 2, 4-(11) and 3, 4-di-O-methyl-α-D-fucopyranosides (8) were prepared from methyl α-D-fucopyranoside via methyl 3, 4-O-isopropylidene-α-D-fucopyranoside. These substances were required in connection with methylation analysis of saponins containing D-fucose residues. Compounds 8 and 11 had not previously been synthesized at the outset of the present work. |
doi_str_mv | 10.1248/cpb.28.632 |
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These substances were required in connection with methylation analysis of saponins containing D-fucose residues. 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Pharm. Bull.</addtitle><description>Methyl 2, 3-(15), 2, 4-(11) and 3, 4-di-O-methyl-α-D-fucopyranosides (8) were prepared from methyl α-D-fucopyranoside via methyl 3, 4-O-isopropylidene-α-D-fucopyranoside. These substances were required in connection with methylation analysis of saponins containing D-fucose residues. Compounds 8 and 11 had not previously been synthesized at the outset of the present work.</description><subject>methylation</subject><issn>0009-2363</issn><issn>1347-5223</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1980</creationdate><recordtype>article</recordtype><recordid>eNpFkMtOwzAQRS0EEuWx4QuyRnWxZ5LYXqKW8lBRF8A6cu0JTVWSyg6LfBY_wjeRKAg2c0e6Z2ZxGLuSYiYh1TfusJmBnuUIR2wiMVU8A8BjNhFCGA6Y4yk7i3EnBGRC4YQ9vXR1u6VYxaQpk2dqt90-gWmCfDpEyhNb-wSHbVHxNR8J_v3FF3z56ZpDF2zdxMpTvGAnpd1HuvzNc_a2vHudP_DV-v5xfrviLhUKuDLe5xtrcklKKg1pSloQ2az0CiBXqN3GOkOAmHptEEiKHIzOLFoqvcVzdj3-daGJMVBZHEL1YUNXSFEMForeQgG66C308HyEd7G17_SH2tBWbk8DKk2mBxzG0V_9t1sbCqrxBwXNZGM</recordid><startdate>1980</startdate><enddate>1980</enddate><creator>TAKEDA, TADAHIRO</creator><creator>TAKABE, SEIICHI</creator><creator>OGIHARA, YUKIO</creator><general>The Pharmaceutical Society of Japan</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>1980</creationdate><title>Synthesis of Methyl 2, 3-, 2, 4- and 3, 4-Di-O-Methyl-α-D-Fucopyranosides</title><author>TAKEDA, TADAHIRO ; TAKABE, SEIICHI ; OGIHARA, YUKIO</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4072-79dd6ba961e7178244e80eea5fd7226738cbac9e2334d8932e1062985a3aefda3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1980</creationdate><topic>methylation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>TAKEDA, TADAHIRO</creatorcontrib><creatorcontrib>TAKABE, SEIICHI</creatorcontrib><creatorcontrib>OGIHARA, YUKIO</creatorcontrib><collection>CrossRef</collection><jtitle>Chemical & pharmaceutical bulletin</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>TAKEDA, TADAHIRO</au><au>TAKABE, SEIICHI</au><au>OGIHARA, YUKIO</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Methyl 2, 3-, 2, 4- and 3, 4-Di-O-Methyl-α-D-Fucopyranosides</atitle><jtitle>Chemical & pharmaceutical bulletin</jtitle><addtitle>Chem. Pharm. Bull.</addtitle><date>1980</date><risdate>1980</risdate><volume>28</volume><issue>2</issue><spage>632</spage><epage>634</epage><pages>632-634</pages><issn>0009-2363</issn><eissn>1347-5223</eissn><abstract>Methyl 2, 3-(15), 2, 4-(11) and 3, 4-di-O-methyl-α-D-fucopyranosides (8) were prepared from methyl α-D-fucopyranoside via methyl 3, 4-O-isopropylidene-α-D-fucopyranoside. These substances were required in connection with methylation analysis of saponins containing D-fucose residues. Compounds 8 and 11 had not previously been synthesized at the outset of the present work.</abstract><pub>The Pharmaceutical Society of Japan</pub><doi>10.1248/cpb.28.632</doi><tpages>3</tpages><oa>free_for_read</oa></addata></record> |
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source | J-STAGE Free; EZB-FREE-00999 freely available EZB journals; Free Full-Text Journals in Chemistry |
subjects | methylation |
title | Synthesis of Methyl 2, 3-, 2, 4- and 3, 4-Di-O-Methyl-α-D-Fucopyranosides |
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