ZnO/ZnAl 2 O 4 Nanocomposite Films Studied by X-Ray Diffraction, FTIR, and X-Ray Photoelectron Spectroscopy
ZnO/ZnAl 2 O 4 nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by extracting Al 2 O(SO 4 ) 2 oxide with zinc chloride hydrate in deionised water. The sample was then subjected to heat treatment at 650°C and 700°C for 1 h, which led to the formation of the spinel oxide (ZnAl...
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| Veröffentlicht in: | Journal of spectroscopy (Hindawi) 2015, Vol.2015, p.1-9 |
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| container_title | Journal of spectroscopy (Hindawi) |
| container_volume | 2015 |
| creator | Iaiche, S. Djelloul, A. |
| description | ZnO/ZnAl
2
O
4
nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by extracting Al
2
O(SO
4
)
2
oxide with zinc chloride hydrate in deionised water. The sample was then subjected to heat treatment at 650°C and 700°C for 1 h, which led to the formation of the spinel oxide (ZnAl
2
O
4
) and wurtzite (ZnO) phases. Al
2
(SO
4
)
3
·18H
2
O salt was transformed into aluminum oxide sulfate Al
2
O(SO
4
)
2
, which is an intermediary decomposition product, by calcination at 795°C for 3 h. The structures of the synthesised ZnO/ZnAl
2
O
4
films were confirmed by XRD, FTIR, and X-ray photoelectron spectroscopy (XPS). XPS spectra of the major Zn, Al, and O photoelectron lines and the major X-ray induced Zn LMM Auger lines for ZnO/ZnAl
2
O
4
are presented. |
| doi_str_mv | 10.1155/2015/836859 |
| format | Article |
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2
O
4
nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by extracting Al
2
O(SO
4
)
2
oxide with zinc chloride hydrate in deionised water. The sample was then subjected to heat treatment at 650°C and 700°C for 1 h, which led to the formation of the spinel oxide (ZnAl
2
O
4
) and wurtzite (ZnO) phases. Al
2
(SO
4
)
3
·18H
2
O salt was transformed into aluminum oxide sulfate Al
2
O(SO
4
)
2
, which is an intermediary decomposition product, by calcination at 795°C for 3 h. The structures of the synthesised ZnO/ZnAl
2
O
4
films were confirmed by XRD, FTIR, and X-ray photoelectron spectroscopy (XPS). XPS spectra of the major Zn, Al, and O photoelectron lines and the major X-ray induced Zn LMM Auger lines for ZnO/ZnAl
2
O
4
are presented.</description><identifier>ISSN: 2314-4920</identifier><identifier>EISSN: 2314-4939</identifier><identifier>DOI: 10.1155/2015/836859</identifier><language>eng</language><ispartof>Journal of spectroscopy (Hindawi), 2015, Vol.2015, p.1-9</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c789-673f035ae45cac6e5a1a2154de066a6f4bf34032a20084ada53b8efb783a4c813</citedby><cites>FETCH-LOGICAL-c789-673f035ae45cac6e5a1a2154de066a6f4bf34032a20084ada53b8efb783a4c813</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,860,4010,27900,27901,27902</link.rule.ids></links><search><creatorcontrib>Iaiche, S.</creatorcontrib><creatorcontrib>Djelloul, A.</creatorcontrib><title>ZnO/ZnAl 2 O 4 Nanocomposite Films Studied by X-Ray Diffraction, FTIR, and X-Ray Photoelectron Spectroscopy</title><title>Journal of spectroscopy (Hindawi)</title><description>ZnO/ZnAl
2
O
4
nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by extracting Al
2
O(SO
4
)
2
oxide with zinc chloride hydrate in deionised water. The sample was then subjected to heat treatment at 650°C and 700°C for 1 h, which led to the formation of the spinel oxide (ZnAl
2
O
4
) and wurtzite (ZnO) phases. Al
2
(SO
4
)
3
·18H
2
O salt was transformed into aluminum oxide sulfate Al
2
O(SO
4
)
2
, which is an intermediary decomposition product, by calcination at 795°C for 3 h. The structures of the synthesised ZnO/ZnAl
2
O
4
films were confirmed by XRD, FTIR, and X-ray photoelectron spectroscopy (XPS). XPS spectra of the major Zn, Al, and O photoelectron lines and the major X-ray induced Zn LMM Auger lines for ZnO/ZnAl
2
O
4
are presented.</description><issn>2314-4920</issn><issn>2314-4939</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNo9kE1Lw0AQhhdRsNSe_AN7tzH7mWyOpVotFCNtDtJLmGx2MZpkQzYe8u9NbfH0PvAOM8OD0D0lj5RKGTJCZah4pGRyhWaMUxGIhCfX_8zILVp4_0XINCmYSOQMfR_bNDy2qxoznGKB36B12jWd89Vg8KaqG48Pw09ZmRIXI_4I9jDip8raHvRQuXaJN9l2v8TQlpfy_dMNztRGD71r8aH7A69dN96hGwu1N4tLzlG2ec7Wr8EufdmuV7tAxyoJophbwiUYITXoyEigwKZ_S0OiCCIrCssF4QwYIUpACZIXytgiVhyEVpTP0cN5rZ7u-t7YvOurBvoxpyQ_mcpPpvKzKf4LnRFZbw</recordid><startdate>2015</startdate><enddate>2015</enddate><creator>Iaiche, S.</creator><creator>Djelloul, A.</creator><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>2015</creationdate><title>ZnO/ZnAl 2 O 4 Nanocomposite Films Studied by X-Ray Diffraction, FTIR, and X-Ray Photoelectron Spectroscopy</title><author>Iaiche, S. ; Djelloul, A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c789-673f035ae45cac6e5a1a2154de066a6f4bf34032a20084ada53b8efb783a4c813</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Iaiche, S.</creatorcontrib><creatorcontrib>Djelloul, A.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of spectroscopy (Hindawi)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Iaiche, S.</au><au>Djelloul, A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>ZnO/ZnAl 2 O 4 Nanocomposite Films Studied by X-Ray Diffraction, FTIR, and X-Ray Photoelectron Spectroscopy</atitle><jtitle>Journal of spectroscopy (Hindawi)</jtitle><date>2015</date><risdate>2015</risdate><volume>2015</volume><spage>1</spage><epage>9</epage><pages>1-9</pages><issn>2314-4920</issn><eissn>2314-4939</eissn><abstract>ZnO/ZnAl
2
O
4
nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by extracting Al
2
O(SO
4
)
2
oxide with zinc chloride hydrate in deionised water. The sample was then subjected to heat treatment at 650°C and 700°C for 1 h, which led to the formation of the spinel oxide (ZnAl
2
O
4
) and wurtzite (ZnO) phases. Al
2
(SO
4
)
3
·18H
2
O salt was transformed into aluminum oxide sulfate Al
2
O(SO
4
)
2
, which is an intermediary decomposition product, by calcination at 795°C for 3 h. The structures of the synthesised ZnO/ZnAl
2
O
4
films were confirmed by XRD, FTIR, and X-ray photoelectron spectroscopy (XPS). XPS spectra of the major Zn, Al, and O photoelectron lines and the major X-ray induced Zn LMM Auger lines for ZnO/ZnAl
2
O
4
are presented.</abstract><doi>10.1155/2015/836859</doi><tpages>9</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 2314-4920 |
| ispartof | Journal of spectroscopy (Hindawi), 2015, Vol.2015, p.1-9 |
| issn | 2314-4920 2314-4939 |
| language | eng |
| recordid | cdi_crossref_primary_10_1155_2015_836859 |
| source | Wiley-Blackwell Open Access Titles; DOAJ Directory of Open Access Journals; Alma/SFX Local Collection |
| title | ZnO/ZnAl 2 O 4 Nanocomposite Films Studied by X-Ray Diffraction, FTIR, and X-Ray Photoelectron Spectroscopy |
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