Direct Fabrication of Cobalt Oxide Nanoparticles Employing Sucrose as a Combustion Fuel

Direct Fabrication of Cobalt Oxide Nanoparticles Employing Sucrose as a Combustion Fuel

Combustion method has been used as a fast and facile method to prepare nanocrystalline Co3O4 spinel employing sucrose as a combustion fuel. The products were characterized by thermal analyses (TGA and DTA), X-ray diffraction technique (XRD), Fourier transform infrared spectroscopy (FTIR), scanning e...

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Veröffentlicht in:Journal of Nanoparticles 2013-03, Vol.2013 (2013), p.1-7
Hauptverfasser: Makhlouf, M. Th, Abu-Zied, B. M., Mansoure, T. H.
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container_title Journal of Nanoparticles
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creator Makhlouf, M. Th
Abu-Zied, B. M.
Mansoure, T. H.
description Combustion method has been used as a fast and facile method to prepare nanocrystalline Co3O4 spinel employing sucrose as a combustion fuel. The products were characterized by thermal analyses (TGA and DTA), X-ray diffraction technique (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) techniques. Experimental results revealed that the molar ratio of fuel/oxidizer (F/O) plays an important role in controlling the crystallite size of Co3O4 nanoparticles. Transmission electron microscopy indicated that the crystallite size of Co3O4 nanocrystals was in the range of 13–32 nm. X-ray diffraction confirmed the formation of CoO phase with spinel Co3O4. The effect of calcination temperature on crystallite size and morphology has been, also, discussed.
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