Aluminum Anodization in Deionized Water as Electrolyte

Aluminum Anodization in Deionized Water as Electrolyte

Thin oxide films were prepared electrochemically on the aluminum surface using the high-voltage discharge and potentiostatic methods in deionized water as an electrolyte. The growth of continuous films occurred only at potentials lower than the breakdown potential. The films obtained by the discharg...

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Veröffentlicht in:Journal of the Electrochemical Society 2016-01, Vol.163 (7), p.C364-C368
Hauptverfasser: Lisenkov, Aleksey D., Poznyak, Sergey K., Zheludkevich, Mikhail L., Ferreira, Mário G. S.
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container_end_page C368
container_issue 7
container_start_page C364
container_title Journal of the Electrochemical Society
container_volume 163
creator Lisenkov, Aleksey D.
Poznyak, Sergey K.
Zheludkevich, Mikhail L.
Ferreira, Mário G. S.
description Thin oxide films were prepared electrochemically on the aluminum surface using the high-voltage discharge and potentiostatic methods in deionized water as an electrolyte. The growth of continuous films occurred only at potentials lower than the breakdown potential. The films obtained by the discharge method are more uniform and can grow to a higher thickness in comparison to those formed by the potentiostatic mode, as demonstrated by electrochemical impedance spectroscopy (EIS), transmission electron microscopy (TEM), and scanning Kelvin probe force microscopy (SKPFM). The data herein obtained can be used as a reference to understand better the properties of the films produced in conventional electrolytes where apart from water other species are present.
doi_str_mv 10.1149/2.0881607jes
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