Microstructure Observation of Ni/YSZ Boundary by TEM and STEM
Solid oxide fuel cell attracts much attention due to its advantages such as high efficiency and low carbon emission. For a typical Ni/YSZ anode, it is essential to understand the relationship between performance and microstructure of Ni/YSZ interface and Ni/YSZ/pore triple-phase boundary. Herein, th...
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Veröffentlicht in: | ECS transactions 2013-01, Vol.57 (1), p.1401-1405 |
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description | Solid oxide fuel cell attracts much attention due to its advantages such as high efficiency and low carbon emission. For a typical Ni/YSZ anode, it is essential to understand the relationship between performance and microstructure of Ni/YSZ interface and Ni/YSZ/pore triple-phase boundary. Herein, the crystallographic orientation relationship between Ni and YSZ in a practical cell was investigated by transmission electron microscopy (TEM), and scanning TEM (STEM). The TEM specimen was lifted out from bulk cell in a focused ion beam-scanning electron microscopy. It was found that the orientation relationship is much more complicated than that of a specially designed Ni/YSZ sample. |
doi_str_mv | 10.1149/05701.1401ecst |
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For a typical Ni/YSZ anode, it is essential to understand the relationship between performance and microstructure of Ni/YSZ interface and Ni/YSZ/pore triple-phase boundary. Herein, the crystallographic orientation relationship between Ni and YSZ in a practical cell was investigated by transmission electron microscopy (TEM), and scanning TEM (STEM). The TEM specimen was lifted out from bulk cell in a focused ion beam-scanning electron microscopy. 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For a typical Ni/YSZ anode, it is essential to understand the relationship between performance and microstructure of Ni/YSZ interface and Ni/YSZ/pore triple-phase boundary. Herein, the crystallographic orientation relationship between Ni and YSZ in a practical cell was investigated by transmission electron microscopy (TEM), and scanning TEM (STEM). The TEM specimen was lifted out from bulk cell in a focused ion beam-scanning electron microscopy. It was found that the orientation relationship is much more complicated than that of a specially designed Ni/YSZ sample.</abstract><pub>The Electrochemical Society, Inc</pub><doi>10.1149/05701.1401ecst</doi><tpages>5</tpages></addata></record> |
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title | Microstructure Observation of Ni/YSZ Boundary by TEM and STEM |
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