Wavelength-Dispersive Total Reflection X-Ray Fluorescence with High-Brilliance Undulator Radiation at SPring-8

Wavelength-dispersive total reflection X-ray fluorescence (WD-TXRF) equipment supported by an energy-dispersive (ED) solid-state detector (SSD) has been developed and installed in the BL16XU Industrial Consortium ID Beamline for Material Research at the SPring-8 synchrotron radiation research facili...

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Veröffentlicht in:Japanese Journal of Applied Physics 2000-12, Vol.39 (12A), p.L1252
Hauptverfasser: Awaji, Naoki, Ozaki, Shinji, Nishino, Junichi, Noguchi, Sinichi, Yamamoto, Tohru, Syoji, Takashi, Yamagami, Motoyuki, Kobayashi, Akira, Hirai, You, Shibata, Masahiro, Yamaguchi, Koji, Liu, Kuang-Yu, Kawado, Seiji, Takahashi, Mamoru, Yasuami, Shigeru, Konomi, Ichiro, Kimura, Shigeru, Hirai, Yasuharu, Hasegawa, Masaki, Komiya, Satoshi, Hirose, Takayuki, Okajima, Toshihiro
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container_issue 12A
container_start_page L1252
container_title Japanese Journal of Applied Physics
container_volume 39
creator Awaji, Naoki
Ozaki, Shinji
Nishino, Junichi
Noguchi, Sinichi
Yamamoto, Tohru
Syoji, Takashi
Yamagami, Motoyuki
Kobayashi, Akira
Hirai, You
Shibata, Masahiro
Yamaguchi, Koji
Liu, Kuang-Yu
Kawado, Seiji
Takahashi, Mamoru
Yasuami, Shigeru
Konomi, Ichiro
Kimura, Shigeru
Hirai, Yasuharu
Hasegawa, Masaki
Komiya, Satoshi
Hirose, Takayuki
Okajima, Toshihiro
description Wavelength-dispersive total reflection X-ray fluorescence (WD-TXRF) equipment supported by an energy-dispersive (ED) solid-state detector (SSD) has been developed and installed in the BL16XU Industrial Consortium ID Beamline for Material Research at the SPring-8 synchrotron radiation research facility. Equipment specifications are given and results from our initial experiment are discussed in this paper. In the experiment on the sensitivity of detection of metallic impurities on a Si wafer, the lower limit of detection (LLD) using a Ge-SSD reached an order of 10 8 atoms/cm 2 with a corresponding absolute weight of approximately 10 fg for ED-TXRF. In comparison, an order of 10 9 atoms/cm 2 with a corresponding weight of around 100 fg was obtained for WD-TXRF for the first time. Although ED-TXRF still has a lower LLD, using WD-TXRF can provide good energy resolution with a high count rate, opening up a new field of X-ray fluorescence measurement.
doi_str_mv 10.1143/JJAP.39.L1252
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title Wavelength-Dispersive Total Reflection X-Ray Fluorescence with High-Brilliance Undulator Radiation at SPring-8
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