Method of synthesis and structure of (5E)-5-(2-alkoxy-2-oxoethylidene)-4-hydroxy-2,2-dimethyl-1-(4-methylphenyl)-2,5-dihydro-1H-pyrrole-3-carboxylates
A procedure has been developed for the synthesis of dialkyl (5 E )-5-(2-alkoxy-2-oxoethylidene)-4-hydroxy-2,2-dimethyl-1-(4-methylphenyl)-2,5-dihydro-1 H -pyrrole-3-carboxylates by three-component condensation of dialkyl 3,4-dihydroxyhexa-2,4-dienedioate with acetone and p -toluidine. The structure...
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| Veröffentlicht in: | Russian journal of organic chemistry 2015-06, Vol.51 (6), p.860-863 |
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| container_end_page | 863 |
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| container_issue | 6 |
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| container_title | Russian journal of organic chemistry |
| container_volume | 51 |
| creator | Mukovoz, P. P. Koz’minykh, V. O. Andreeva, V. A. El’tsov, O. S. Slepukhin, P. A. Koz’minykh, E. N. |
| description | A procedure has been developed for the synthesis of dialkyl (5
E
)-5-(2-alkoxy-2-oxoethylidene)-4-hydroxy-2,2-dimethyl-1-(4-methylphenyl)-2,5-dihydro-1
H
-pyrrole-3-carboxylates by three-component condensation of dialkyl 3,4-dihydroxyhexa-2,4-dienedioate with acetone and
p
-toluidine. The structure of the products is discussed on the basis of the IR,
1
H NMR, and X-ray diffraction data. |
| doi_str_mv | 10.1134/S107042801506007X |
| format | Article |
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-pyrrole-3-carboxylates by three-component condensation of dialkyl 3,4-dihydroxyhexa-2,4-dienedioate with acetone and
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E
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H
-pyrrole-3-carboxylates by three-component condensation of dialkyl 3,4-dihydroxyhexa-2,4-dienedioate with acetone and
p
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1
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E
)-5-(2-alkoxy-2-oxoethylidene)-4-hydroxy-2,2-dimethyl-1-(4-methylphenyl)-2,5-dihydro-1
H
-pyrrole-3-carboxylates by three-component condensation of dialkyl 3,4-dihydroxyhexa-2,4-dienedioate with acetone and
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1
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| subjects | Chemistry Chemistry and Materials Science Organic Chemistry |
| title | Method of synthesis and structure of (5E)-5-(2-alkoxy-2-oxoethylidene)-4-hydroxy-2,2-dimethyl-1-(4-methylphenyl)-2,5-dihydro-1H-pyrrole-3-carboxylates |
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