Features of the synthesis of unsaturated sulfides proceeding from (2-chloroprop-2-en-1-yl)isothiouronium chloride
Procedure of synthesis of sulfides containing a chloropropenyl fragment sensitive to bases was modified. The change in the sequence of reagents addition ensuring a contact of isothiouronium salt with a minimal base quantity and the application of a mixture hydrazine hydrate-alkali allowed the prepar...
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| Veröffentlicht in: | Russian journal of organic chemistry 2015-02, Vol.51 (2), p.161-166 |
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| container_end_page | 166 |
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| container_issue | 2 |
| container_start_page | 161 |
| container_title | Russian journal of organic chemistry |
| container_volume | 51 |
| creator | Levanova, E. P. Vakhrina, V. S. Grabel’nykh, V. A. Rozentsveig, I. B. Russavskaya, N. V. Albanov, A. I. Sanzheeva, E. R. Korchevin, N. A. |
| description | Procedure of synthesis of sulfides containing a chloropropenyl fragment sensitive to bases was modified. The change in the sequence of reagents addition ensuring a contact of isothiouronium salt with a minimal base quantity and the application of a mixture hydrazine hydrate-alkali allowed the preparation of target sulfides under mild conditions in up to 93% yields. |
| doi_str_mv | 10.1134/S1070428015020037 |
| format | Article |
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| subjects | Chemistry Chemistry and Materials Science Organic Chemistry |
| title | Features of the synthesis of unsaturated sulfides proceeding from (2-chloroprop-2-en-1-yl)isothiouronium chloride |
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