Mesoporous MgO: Synthesis, physico-chemical, and catalytic properties
Mesoporous MgO was obtained via the hydrothermal synthesis using both ionogenic and non-ionogenic surfactants as structure-directing templates. The materials prepared were characterized by SEM, BET-N 2 , XRD, and TG-DTA techniques. MgO particles are spherical 20-μm aggregates of primary oxide partic...
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| Veröffentlicht in: | Russian Journal of Physical Chemistry A 2016-06, Vol.90 (6), p.1212-1216 |
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| container_title | Russian Journal of Physical Chemistry A |
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| creator | Maerle, A. A. Kasyanov, I. A. Moskovskaya, I. F. Romanovsky, B. V. |
| description | Mesoporous MgO was obtained via the hydrothermal synthesis using both ionogenic and non-ionogenic surfactants as structure-directing templates. The materials prepared were characterized by SEM, BET-N
2
, XRD, and TG-DTA techniques. MgO particles are spherical 20-μm aggregates of primary oxide particles well shaped as rectangular parallelepipeds. Magnesium oxide samples have the specific surface area of 290–400 m
2
/g and pore sizes of 3.3–4.1 nm. Their mesoporous structure remained unchanged after calcination up to 350°C. Catalytic activity of mesoporous MgO was studied in acetone condensation reaction. |
| doi_str_mv | 10.1134/S0036024416060108 |
| format | Article |
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2
, XRD, and TG-DTA techniques. MgO particles are spherical 20-μm aggregates of primary oxide particles well shaped as rectangular parallelepipeds. Magnesium oxide samples have the specific surface area of 290–400 m
2
/g and pore sizes of 3.3–4.1 nm. Their mesoporous structure remained unchanged after calcination up to 350°C. Catalytic activity of mesoporous MgO was studied in acetone condensation reaction.</description><identifier>ISSN: 0036-0244</identifier><identifier>EISSN: 1531-863X</identifier><identifier>DOI: 10.1134/S0036024416060108</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Chemistry ; Chemistry and Materials Science ; Physical Chemistry ; Physical Chemistry of Nanoclusters and Nanomaterials</subject><ispartof>Russian Journal of Physical Chemistry A, 2016-06, Vol.90 (6), p.1212-1216</ispartof><rights>Pleiades Publishing, Ltd. 2016</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c288t-b647ec2503542346ce91ebf16149ae14acf255562955ad7f1e066a456d67e7763</citedby><cites>FETCH-LOGICAL-c288t-b647ec2503542346ce91ebf16149ae14acf255562955ad7f1e066a456d67e7763</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0036024416060108$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0036024416060108$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Maerle, A. A.</creatorcontrib><creatorcontrib>Kasyanov, I. A.</creatorcontrib><creatorcontrib>Moskovskaya, I. F.</creatorcontrib><creatorcontrib>Romanovsky, B. V.</creatorcontrib><title>Mesoporous MgO: Synthesis, physico-chemical, and catalytic properties</title><title>Russian Journal of Physical Chemistry A</title><addtitle>Russ. J. Phys. Chem</addtitle><description>Mesoporous MgO was obtained via the hydrothermal synthesis using both ionogenic and non-ionogenic surfactants as structure-directing templates. The materials prepared were characterized by SEM, BET-N
2
, XRD, and TG-DTA techniques. MgO particles are spherical 20-μm aggregates of primary oxide particles well shaped as rectangular parallelepipeds. Magnesium oxide samples have the specific surface area of 290–400 m
2
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2
, XRD, and TG-DTA techniques. MgO particles are spherical 20-μm aggregates of primary oxide particles well shaped as rectangular parallelepipeds. Magnesium oxide samples have the specific surface area of 290–400 m
2
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| subjects | Chemistry Chemistry and Materials Science Physical Chemistry Physical Chemistry of Nanoclusters and Nanomaterials |
| title | Mesoporous MgO: Synthesis, physico-chemical, and catalytic properties |
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