Synthesis and some properties of Nd(B11H14)3 · 4Dg (Dg is diglyme)

The reaction of Nd(BH 4 ) 3 · 3THF with decaborane-14 in diglyme at 85–90°C yields Nd(B 11 H 14 ) 3 · 4Dg. The duration of the reaction is 20 h. The molar ratio of Nd(BH 4 ) 3 · 3THF to B 10 H 14 is is 1 :3.5. The product is precipitated with heptane from a diglyme solution. The yield is 70%. In an...

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Veröffentlicht in:	Russian journal of inorganic chemistry 2008, Vol.53 (4), p.565-567
Hauptverfasser:	Titov, L. V., Gavrilova, L. A., Petrovskii, P. V.
Format:	Artikel
Sprache:	eng
Schlagworte:	Chemistry Chemistry and Materials Science Coordination Compounds Inorganic Chemistry
Online-Zugang:	Volltext
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