Crystal structures of 4-(oxiran-2-ylmethoxy) benzoic acid and 4-acetoxybenzoic acid
Compounds 4-(oxiran-2-ylmethoxy)benzoic acid ( 2 ) and 4-acetoxybenzoic acid ( 4 ) are synthesized by a new synthetic route and studied by X-ray crystallography. Compound 2 crystallizes in the monoclinic system, P 2 1 / n space group, a = 5.1209(2) Å, b = 30.3429(16) Å, c = 5.9153(3) Å, β = 96.725(3...
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| Veröffentlicht in: | Journal of structural chemistry 2012-07, Vol.53 (4), p.793-799 |
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| container_title | Journal of structural chemistry |
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| creator | Obreza, A. Perdih, F. |
| description | Compounds 4-(oxiran-2-ylmethoxy)benzoic acid (
2
) and 4-acetoxybenzoic acid (
4
) are synthesized by a new synthetic route and studied by X-ray crystallography. Compound
2
crystallizes in the monoclinic system,
P
2
1
/
n
space group,
a
= 5.1209(2) Å,
b
= 30.3429(16) Å,
c
= 5.9153(3) Å, β = 96.725(3)°,
V
= 912.81(8) Å
3
,
Z
= 4. Compound
4
crystallizes in the triclinic system,
P
-1 space group,
a
= 7.3400(4) Å,
b
= 8.0819(3) Å,
c
= 15.6548(9) Å, α = 85.754(3)°, β = 84.268(2)°, γ = 70.023(3)°,
V
= 867.63(8) Å
3
,
Z
= 4. The crystal structure of
2
comprises two crystallographically independent molecules of the compound. In the crystal structures of
2
and
4
, pairs of molecules form carboxyl dimers. |
| doi_str_mv | 10.1134/S0022476612040257 |
| format | Article |
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2
) and 4-acetoxybenzoic acid (
4
) are synthesized by a new synthetic route and studied by X-ray crystallography. Compound
2
crystallizes in the monoclinic system,
P
2
1
/
n
space group,
a
= 5.1209(2) Å,
b
= 30.3429(16) Å,
c
= 5.9153(3) Å, β = 96.725(3)°,
V
= 912.81(8) Å
3
,
Z
= 4. Compound
4
crystallizes in the triclinic system,
P
-1 space group,
a
= 7.3400(4) Å,
b
= 8.0819(3) Å,
c
= 15.6548(9) Å, α = 85.754(3)°, β = 84.268(2)°, γ = 70.023(3)°,
V
= 867.63(8) Å
3
,
Z
= 4. The crystal structure of
2
comprises two crystallographically independent molecules of the compound. In the crystal structures of
2
and
4
, pairs of molecules form carboxyl dimers.</description><identifier>ISSN: 0022-4766</identifier><identifier>EISSN: 1573-8779</identifier><identifier>DOI: 10.1134/S0022476612040257</identifier><language>eng</language><publisher>Dordrecht: SP MAIK Nauka/Interperiodica</publisher><subject>Atomic ; Atomic/Molecular Structure and Spectra ; Chemistry ; Chemistry and Materials Science ; Inorganic Chemistry ; Molecular ; Optical and Plasma Physics ; Physical Chemistry ; Solid State Physics</subject><ispartof>Journal of structural chemistry, 2012-07, Vol.53 (4), p.793-799</ispartof><rights>Pleiades Publishing, Ltd. 2012</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c288t-6b73261f04f0f4ff879a6239d76ab5a14ed880da6040198f3b568ee0d7c9af43</citedby><cites>FETCH-LOGICAL-c288t-6b73261f04f0f4ff879a6239d76ab5a14ed880da6040198f3b568ee0d7c9af43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0022476612040257$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0022476612040257$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Obreza, A.</creatorcontrib><creatorcontrib>Perdih, F.</creatorcontrib><title>Crystal structures of 4-(oxiran-2-ylmethoxy) benzoic acid and 4-acetoxybenzoic acid</title><title>Journal of structural chemistry</title><addtitle>J Struct Chem</addtitle><description>Compounds 4-(oxiran-2-ylmethoxy)benzoic acid (
2
) and 4-acetoxybenzoic acid (
4
) are synthesized by a new synthetic route and studied by X-ray crystallography. Compound
2
crystallizes in the monoclinic system,
P
2
1
/
n
space group,
a
= 5.1209(2) Å,
b
= 30.3429(16) Å,
c
= 5.9153(3) Å, β = 96.725(3)°,
V
= 912.81(8) Å
3
,
Z
= 4. Compound
4
crystallizes in the triclinic system,
P
-1 space group,
a
= 7.3400(4) Å,
b
= 8.0819(3) Å,
c
= 15.6548(9) Å, α = 85.754(3)°, β = 84.268(2)°, γ = 70.023(3)°,
V
= 867.63(8) Å
3
,
Z
= 4. The crystal structure of
2
comprises two crystallographically independent molecules of the compound. In the crystal structures of
2
and
4
, pairs of molecules form carboxyl dimers.</description><subject>Atomic</subject><subject>Atomic/Molecular Structure and Spectra</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Inorganic Chemistry</subject><subject>Molecular</subject><subject>Optical and Plasma Physics</subject><subject>Physical Chemistry</subject><subject>Solid State Physics</subject><issn>0022-4766</issn><issn>1573-8779</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNp9kE1LxDAQhoMoWFd_gLcc9RCdpGk-jlL8ggUPu_eSpol26baStLD115uyHgTB0xye9xlmXoSuKdxRmvP7DQBjXApBGXBghTxBGS1kTpSU-hRlCyYLP0cXMe4AQCstMrQpwxxH0-E4hsmOU3ARDx5zcjMc2mB6wsjc7d34MRzmW1y7_mtoLTa2bbDpm5Qz1o2J_SaX6MybLrqrn7lC26fHbflC1m_Pr-XDmlim1EhELXMmqAfuwXPvldRGsFw3Upi6MJS7RilojEgPUa18XhdCOQeNtNp4nq8QPa61YYgxOF99hnZvwlxRqJZSqj-lJIcdnZiy_bsL1W6YQp-u_Ef6BvyYY3U</recordid><startdate>20120701</startdate><enddate>20120701</enddate><creator>Obreza, A.</creator><creator>Perdih, F.</creator><general>SP MAIK Nauka/Interperiodica</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20120701</creationdate><title>Crystal structures of 4-(oxiran-2-ylmethoxy) benzoic acid and 4-acetoxybenzoic acid</title><author>Obreza, A. ; Perdih, F.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c288t-6b73261f04f0f4ff879a6239d76ab5a14ed880da6040198f3b568ee0d7c9af43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Atomic</topic><topic>Atomic/Molecular Structure and Spectra</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Inorganic Chemistry</topic><topic>Molecular</topic><topic>Optical and Plasma Physics</topic><topic>Physical Chemistry</topic><topic>Solid State Physics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Obreza, A.</creatorcontrib><creatorcontrib>Perdih, F.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of structural chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Obreza, A.</au><au>Perdih, F.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Crystal structures of 4-(oxiran-2-ylmethoxy) benzoic acid and 4-acetoxybenzoic acid</atitle><jtitle>Journal of structural chemistry</jtitle><stitle>J Struct Chem</stitle><date>2012-07-01</date><risdate>2012</risdate><volume>53</volume><issue>4</issue><spage>793</spage><epage>799</epage><pages>793-799</pages><issn>0022-4766</issn><eissn>1573-8779</eissn><abstract>Compounds 4-(oxiran-2-ylmethoxy)benzoic acid (
2
) and 4-acetoxybenzoic acid (
4
) are synthesized by a new synthetic route and studied by X-ray crystallography. Compound
2
crystallizes in the monoclinic system,
P
2
1
/
n
space group,
a
= 5.1209(2) Å,
b
= 30.3429(16) Å,
c
= 5.9153(3) Å, β = 96.725(3)°,
V
= 912.81(8) Å
3
,
Z
= 4. Compound
4
crystallizes in the triclinic system,
P
-1 space group,
a
= 7.3400(4) Å,
b
= 8.0819(3) Å,
c
= 15.6548(9) Å, α = 85.754(3)°, β = 84.268(2)°, γ = 70.023(3)°,
V
= 867.63(8) Å
3
,
Z
= 4. The crystal structure of
2
comprises two crystallographically independent molecules of the compound. In the crystal structures of
2
and
4
, pairs of molecules form carboxyl dimers.</abstract><cop>Dordrecht</cop><pub>SP MAIK Nauka/Interperiodica</pub><doi>10.1134/S0022476612040257</doi><tpages>7</tpages></addata></record> |
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| ispartof | Journal of structural chemistry, 2012-07, Vol.53 (4), p.793-799 |
| issn | 0022-4766 1573-8779 |
| language | eng |
| recordid | cdi_crossref_primary_10_1134_S0022476612040257 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Atomic Atomic/Molecular Structure and Spectra Chemistry Chemistry and Materials Science Inorganic Chemistry Molecular Optical and Plasma Physics Physical Chemistry Solid State Physics |
| title | Crystal structures of 4-(oxiran-2-ylmethoxy) benzoic acid and 4-acetoxybenzoic acid |
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