Crystal structure of salts of indole alkaloid norfluorocurarine
Single crystal XRD is used to study the crystals of salts of indole alkaloid norfluorocurarine: hydrochloride recrystallized from absolute alcohol, dihydrate hydrochloride recrystallized from water, methochloride monohydrate recrystallized from water, solvate form of methochloride obtained from etha...
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| Veröffentlicht in: | Journal of structural chemistry 2012-05, Vol.53 (3), p.542-547 |
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| container_title | Journal of structural chemistry |
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| creator | Tashkhodzhaev, B. Mirzaeva, M. M. Yuldashev, P. Kh |
| description | Single crystal XRD is used to study the crystals of salts of indole alkaloid norfluorocurarine: hydrochloride recrystallized from absolute alcohol, dihydrate hydrochloride recrystallized from water, methochloride monohydrate recrystallized from water, solvate form of methochloride obtained from ethanol, and methobromide monohydrate. Intra- and intermolecular hydrogen bonds are analyzed in these crystals. The crystal structures of norfluorocurarine methochloride and methobromide monohydrates are isomorphic. In norfluorocurarine salts, the orientation of the carbonyl group is determined by the intramolecular C19=O…H-N1 hydrogen bond that is absent in the solvate form with ethanol. |
| doi_str_mv | 10.1134/S0022476612030183 |
| format | Article |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Atomic Atomic/Molecular Structure and Spectra Chemistry Chemistry and Materials Science Inorganic Chemistry Molecular Optical and Plasma Physics Physical Chemistry Solid State Physics |
| title | Crystal structure of salts of indole alkaloid norfluorocurarine |
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