Construction of a Pb II coordination polymer from a semi-rigid ditopic 2,2-biimidazole derivative: synthesis, crystal structure and characterization
A new Pb coordination polymer, poly[0.75(aqua)[μ -4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoato-κ O,O';N;O'',O''']]lead(II)] 1.25-hydrate], {[Pb(C H N O )(H O) ]·1.25H O} or {[Pb(L)(H O) ]·1.25H O} (1) [H L = 4,4'-(1H,1'H-[2,2'-...
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| Veröffentlicht in: | Acta crystallographica. Section C, Structural chemistry Structural chemistry, 2023-07, Vol.79 (Pt 7), p.263-268 |
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| container_issue | Pt 7 |
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| container_title | Acta crystallographica. Section C, Structural chemistry |
| container_volume | 79 |
| creator | Liu, Xiangning Cai, Hua Zhou, Ruikang Li, Yaqi |
| description | A new Pb
coordination polymer, poly[0.75(aqua)[μ
-4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoato-κ
O,O';N;O'',O''']]lead(II)] 1.25-hydrate], {[Pb(C
H
N
O
)(H
O)
]·1.25H
O}
or {[Pb(L)(H
O)
]·1.25H
O}
(1) [H
L = 4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoic acid], was synthesized under solvothermal reaction conditions and characterized using microanalysis, IR spectroscopy and thermogravimetric analysis. Single-crystal structure analysis reveals that a two-dimensional corrugated layer structure is formed in 1 and that neighbouring layers are further extended into a three-dimensional structure by hydrogen-bonding interactions. In addition, a fluorescence sensing experiment towards Cu
based on the polymeric Pb
complex was carried out. |
| doi_str_mv | 10.1107/S2053229623004783 |
| format | Article |
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coordination polymer, poly[0.75(aqua)[μ
-4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoato-κ
O,O';N;O'',O''']]lead(II)] 1.25-hydrate], {[Pb(C
H
N
O
)(H
O)
]·1.25H
O}
or {[Pb(L)(H
O)
]·1.25H
O}
(1) [H
L = 4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoic acid], was synthesized under solvothermal reaction conditions and characterized using microanalysis, IR spectroscopy and thermogravimetric analysis. Single-crystal structure analysis reveals that a two-dimensional corrugated layer structure is formed in 1 and that neighbouring layers are further extended into a three-dimensional structure by hydrogen-bonding interactions. In addition, a fluorescence sensing experiment towards Cu
based on the polymeric Pb
complex was carried out.</description><identifier>ISSN: 2053-2296</identifier><identifier>EISSN: 2053-2296</identifier><identifier>DOI: 10.1107/S2053229623004783</identifier><identifier>PMID: 37313998</identifier><language>eng</language><publisher>England</publisher><ispartof>Acta crystallographica. Section C, Structural chemistry, 2023-07, Vol.79 (Pt 7), p.263-268</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c658-4981ed1f380bf50622f3f664119226a21961f8e9930a578da3e939fbd0d6719d3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/37313998$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Liu, Xiangning</creatorcontrib><creatorcontrib>Cai, Hua</creatorcontrib><creatorcontrib>Zhou, Ruikang</creatorcontrib><creatorcontrib>Li, Yaqi</creatorcontrib><title>Construction of a Pb II coordination polymer from a semi-rigid ditopic 2,2-biimidazole derivative: synthesis, crystal structure and characterization</title><title>Acta crystallographica. Section C, Structural chemistry</title><addtitle>Acta Crystallogr C Struct Chem</addtitle><description><!?tlsb=-0.04pt>A new Pb
coordination polymer, poly[0.75(aqua)[μ
-4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoato-κ
O,O';N;O'',O''']]lead(II)] 1.25-hydrate], {[Pb(C
H
N
O
)(H
O)
]·1.25H
O}
or {[Pb(L)(H
O)
]·1.25H
O}
(1) [H
L = 4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoic acid], was synthesized under solvothermal reaction conditions and characterized using microanalysis, IR spectroscopy and thermogravimetric analysis. Single-crystal structure analysis reveals that a two-dimensional corrugated layer structure is formed in 1 and that neighbouring layers are further extended into a three-dimensional structure by hydrogen-bonding interactions. In addition, a fluorescence sensing experiment towards Cu
based on the polymeric Pb
complex was carried out.</description><issn>2053-2296</issn><issn>2053-2296</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNplkN1KwzAYhoMoTuYuwBPJBayaL1nTxjMZ_gwGCu68pPlxkbYpSTfo7sNzr8Urcz8qgkffxwvP-8KD0AWQKwCSXb9QkjJKBaeMkEmWsyN0touSXXb85x-gUYxvhBAAmmYZnKIByxgwIfIz9D71TezCSnXON9hbLPFziWczrLwP2jVyn7e-6msTsA2-xvLzI5raJcG9Oo2163zrFKZjmpTO1U7Lja8M1ia49ZZemxsc-6ZbmujiGKvQx05W-LC5CgbLRmO1lEGqbots9oPn6MTKKprR9x2ixf3dYvqYzJ8eZtPbeaJ4micTkYPRYFlOSpsSTqlllvMJgKCUSwqCg82NEIzINMu1ZEYwYUtNNM9AaDZEcKhVwccYjC3a4GoZ-gJIsZNc_JO8ZS4PTLsqa6N_iR-l7At2hXnw</recordid><startdate>20230701</startdate><enddate>20230701</enddate><creator>Liu, Xiangning</creator><creator>Cai, Hua</creator><creator>Zhou, Ruikang</creator><creator>Li, Yaqi</creator><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20230701</creationdate><title>Construction of a Pb II coordination polymer from a semi-rigid ditopic 2,2-biimidazole derivative: synthesis, crystal structure and characterization</title><author>Liu, Xiangning ; Cai, Hua ; Zhou, Ruikang ; Li, Yaqi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c658-4981ed1f380bf50622f3f664119226a21961f8e9930a578da3e939fbd0d6719d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Xiangning</creatorcontrib><creatorcontrib>Cai, Hua</creatorcontrib><creatorcontrib>Zhou, Ruikang</creatorcontrib><creatorcontrib>Li, Yaqi</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><jtitle>Acta crystallographica. Section C, Structural chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Xiangning</au><au>Cai, Hua</au><au>Zhou, Ruikang</au><au>Li, Yaqi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Construction of a Pb II coordination polymer from a semi-rigid ditopic 2,2-biimidazole derivative: synthesis, crystal structure and characterization</atitle><jtitle>Acta crystallographica. Section C, Structural chemistry</jtitle><addtitle>Acta Crystallogr C Struct Chem</addtitle><date>2023-07-01</date><risdate>2023</risdate><volume>79</volume><issue>Pt 7</issue><spage>263</spage><epage>268</epage><pages>263-268</pages><issn>2053-2296</issn><eissn>2053-2296</eissn><abstract><!?tlsb=-0.04pt>A new Pb
coordination polymer, poly[0.75(aqua)[μ
-4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoato-κ
O,O';N;O'',O''']]lead(II)] 1.25-hydrate], {[Pb(C
H
N
O
)(H
O)
]·1.25H
O}
or {[Pb(L)(H
O)
]·1.25H
O}
(1) [H
L = 4,4'-(1H,1'H-[2,2'-biimidazole]-1,1'-diyl)dibenzoic acid], was synthesized under solvothermal reaction conditions and characterized using microanalysis, IR spectroscopy and thermogravimetric analysis. Single-crystal structure analysis reveals that a two-dimensional corrugated layer structure is formed in 1 and that neighbouring layers are further extended into a three-dimensional structure by hydrogen-bonding interactions. In addition, a fluorescence sensing experiment towards Cu
based on the polymeric Pb
complex was carried out.</abstract><cop>England</cop><pmid>37313998</pmid><doi>10.1107/S2053229623004783</doi><tpages>6</tpages></addata></record> |
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| identifier | ISSN: 2053-2296 |
| ispartof | Acta crystallographica. Section C, Structural chemistry, 2023-07, Vol.79 (Pt 7), p.263-268 |
| issn | 2053-2296 2053-2296 |
| language | eng |
| recordid | cdi_crossref_primary_10_1107_S2053229623004783 |
| source | Wiley Journals; Alma/SFX Local Collection |
| title | Construction of a Pb II coordination polymer from a semi-rigid ditopic 2,2-biimidazole derivative: synthesis, crystal structure and characterization |
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