(2R,2′S)‐2,2′‐(Ethane‐1,2‐diyldiiminio)bis(butane‐2,1‐diyl) disulfate dihydrate
The title compound, C10H28N2O10S2, was synthesized by the reaction of concentrated sulfuric acid with (R,S)‐ethambutol. The zwitterionic amino–sulfate system, protonated at both N atoms, lies about a centre of symmetry. The asymmetric unit also contains a solvent water molecule. In the crystal stru...
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Veröffentlicht in: | Acta crystallographica. Section E, Structure reports online Structure reports online, 2007-03, Vol.63 (3), p.o1095-o1096 |
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container_title | Acta crystallographica. Section E, Structure reports online |
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creator | Chen, Yong Bai, Guo‐Yi Zhang, Chen‐Fang Simpson, Jim Peng, Hong‐Wei |
description | The title compound, C10H28N2O10S2, was synthesized by the reaction of concentrated sulfuric acid with (R,S)‐ethambutol. The zwitterionic amino–sulfate system, protonated at both N atoms, lies about a centre of symmetry. The asymmetric unit also contains a solvent water molecule. In the crystal structure, intermolecular O—H⋯N and N—H⋯O hydrogen bonds link the molecules into a three‐dimensional network. |
doi_str_mv | 10.1107/S1600536807003480 |
format | Article |
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The zwitterionic amino–sulfate system, protonated at both N atoms, lies about a centre of symmetry. The asymmetric unit also contains a solvent water molecule. In the crystal structure, intermolecular O—H⋯N and N—H⋯O hydrogen bonds link the molecules into a three‐dimensional network.</description><identifier>ISSN: 1600-5368</identifier><identifier>EISSN: 1600-5368</identifier><identifier>DOI: 10.1107/S1600536807003480</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: Blackwell Publishing Ltd</publisher><ispartof>Acta crystallographica. 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Section E, Structure reports online</title><description>The title compound, C10H28N2O10S2, was synthesized by the reaction of concentrated sulfuric acid with (R,S)‐ethambutol. The zwitterionic amino–sulfate system, protonated at both N atoms, lies about a centre of symmetry. The asymmetric unit also contains a solvent water molecule. In the crystal structure, intermolecular O—H⋯N and N—H⋯O hydrogen bonds link the molecules into a three‐dimensional network.</description><issn>1600-5368</issn><issn>1600-5368</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNqFkMFKw0AURQdRsFY_wJ3LFhp972VmklmWEq0QEKwuXIVJZ0JH0lYyLZJdP6Hf4if1S0xMF4ILV-9wL_fyuIxdI9wiQnQ3QwkgQhlDBBDyGE5Yr5WCVjv9xefswvt3AJQRYY9lA3oe0WH3NRsednv6wQYGyWahV7YhbKW9cXVpnFu6lVsPc-cH-XbT-TTCoz-8Mc5vy0JvbEOL2lQNXbKzQpfeXh1vn73eJy-TaZA-PTxOxmkwJx7JQCuMOReqecqGEkOD2qKkvBDIjYiFNTLnwvK5iXMgQJLGGLIgSCkjtQ37DLveebX2vrJF9lG5pa7qDCFrF8r-LNRkVJf5dKWt_w9k47eE0imRkuE3E3puGg</recordid><startdate>200703</startdate><enddate>200703</enddate><creator>Chen, Yong</creator><creator>Bai, Guo‐Yi</creator><creator>Zhang, Chen‐Fang</creator><creator>Simpson, Jim</creator><creator>Peng, Hong‐Wei</creator><general>Blackwell Publishing Ltd</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>200703</creationdate><title>(2R,2′S)‐2,2′‐(Ethane‐1,2‐diyldiiminio)bis(butane‐2,1‐diyl) disulfate dihydrate</title><author>Chen, Yong ; Bai, Guo‐Yi ; Zhang, Chen‐Fang ; Simpson, Jim ; Peng, Hong‐Wei</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2476-a9184459672e3613d1ae162bf514d585ed6b45e4cd8b020126ddd2e05299d6ae3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Chen, Yong</creatorcontrib><creatorcontrib>Bai, Guo‐Yi</creatorcontrib><creatorcontrib>Zhang, Chen‐Fang</creatorcontrib><creatorcontrib>Simpson, Jim</creatorcontrib><creatorcontrib>Peng, Hong‐Wei</creatorcontrib><collection>CrossRef</collection><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Chen, Yong</au><au>Bai, Guo‐Yi</au><au>Zhang, Chen‐Fang</au><au>Simpson, Jim</au><au>Peng, Hong‐Wei</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>(2R,2′S)‐2,2′‐(Ethane‐1,2‐diyldiiminio)bis(butane‐2,1‐diyl) disulfate dihydrate</atitle><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle><date>2007-03</date><risdate>2007</risdate><volume>63</volume><issue>3</issue><spage>o1095</spage><epage>o1096</epage><pages>o1095-o1096</pages><issn>1600-5368</issn><eissn>1600-5368</eissn><abstract>The title compound, C10H28N2O10S2, was synthesized by the reaction of concentrated sulfuric acid with (R,S)‐ethambutol. The zwitterionic amino–sulfate system, protonated at both N atoms, lies about a centre of symmetry. The asymmetric unit also contains a solvent water molecule. In the crystal structure, intermolecular O—H⋯N and N—H⋯O hydrogen bonds link the molecules into a three‐dimensional network.</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1107/S1600536807003480</doi></addata></record> |
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title | (2R,2′S)‐2,2′‐(Ethane‐1,2‐diyldiiminio)bis(butane‐2,1‐diyl) disulfate dihydrate |
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