One-Pot Synthesis of 1-Alkynylphosphonates

One-Pot Synthesis of 1-Alkynylphosphonates

1-Alkynylphosphonates 3 are prepared in a one-pot procedure from diethyl phosphorochloridates 2 and alkynyllithiums 1, which are readily generated by the reaction of 1-alkynes with n-BuLi.

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Synthetic communications 1997-09, Vol.27 (18), p.3171-3174
Hauptverfasser: Gil, Jun Mo, Sung, Jin Wuk, Park, Chan Pil, Oh, Dong Young
Format: Artikel
Sprache:eng
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
Beschreibung
Zusammenfassung:1-Alkynylphosphonates 3 are prepared in a one-pot procedure from diethyl phosphorochloridates 2 and alkynyllithiums 1, which are readily generated by the reaction of 1-alkynes with n-BuLi.
ISSN:0039-7911
1532-2432
DOI:10.1080/00397919708004175