Chirality-directed co-crystallization of different configurationally opposite dialkyl 2,5-diazabicyclo[2.2.2]octane-3,6-dione-1,4-dicarboxylates

Chirality-directed co-crystallization of different configurationally opposite dialkyl 2,5-diazabicyclo[2.2.2]octane-3,6-dione-1,4-dicarboxylates

The title procedure gives quasi-racemic optically active (CD) co-crystals of 4 (space group P21) and 5 of the 1:1 composition; in [CD(–)230]-4, molecules of (–)-1 and (+)-2 are joined by amide H-bonds into infinite linear zigzag tapes packed as infinite columns.

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Veröffentlicht in:Mendeleev communications 1999, Vol.9 (4), p.154-156
Hauptverfasser: Kostyanovsky, Remir G., Lyssenko, Konstantin A., Lenev, Denis A.
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container_title Mendeleev communications
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creator Kostyanovsky, Remir G.
Lyssenko, Konstantin A.
Lenev, Denis A.
description The title procedure gives quasi-racemic optically active (CD) co-crystals of 4 (space group P21) and 5 of the 1:1 composition; in [CD(–)230]-4, molecules of (–)-1 and (+)-2 are joined by amide H-bonds into infinite linear zigzag tapes packed as infinite columns.
doi_str_mv 10.1070/MC1999v009n04ABEH001120
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title Chirality-directed co-crystallization of different configurationally opposite dialkyl 2,5-diazabicyclo[2.2.2]octane-3,6-dione-1,4-dicarboxylates
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