Use of fcc Metals as Internal Temperature Standards in X-Ray Diffraction
A clear pattern of systematic error is found in thermal expansion values for Al, Ag, and Au commonly recommended and used as internal references for temperature determination in x-ray diffraction. Evidence comes from a critical analysis of the literature, including several studies of temperature mea...
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Veröffentlicht in: | Journal of applied physics 1970-04, Vol.41 (5), p.2235-2240 |
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description | A clear pattern of systematic error is found in thermal expansion values for Al, Ag, and Au commonly recommended and used as internal references for temperature determination in x-ray diffraction. Evidence comes from a critical analysis of the literature, including several studies of temperature measurement errors in powder cameras, and from new calibration of a thermometer used previously in precise lattice and length expansion studies. Necessary changes in the commonly accepted values for expansion of Pt and MgO are implied. |
doi_str_mv | 10.1063/1.1659193 |
format | Article |
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title | Use of fcc Metals as Internal Temperature Standards in X-Ray Diffraction |
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