A high temperature furnace for in situ and time-resolved x-ray diffraction studies

A high temperature furnace for in situ and time-resolved x-ray diffraction studies

A high temperature furnace has been built and mounted on a six-circle goniometer for in situ diffraction studies of polycrystalline and powder samples. Temperatures up to 1400 K are controlled with a stability better than ±0.05 K in a vacuum better than 10 −7   atm . The furnace is also able to work...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Review of scientific instruments 1999-05, Vol.70 (5), p.2248-2252
Hauptverfasser: Capitán, M. J., Thouin, N., Rostaing, G.
Format: Artikel
Sprache:eng
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 2252
container_issue 5
container_start_page 2248
container_title Review of scientific instruments
container_volume 70
creator Capitán, M. J.
Thouin, N.
Rostaing, G.
description A high temperature furnace has been built and mounted on a six-circle goniometer for in situ diffraction studies of polycrystalline and powder samples. Temperatures up to 1400 K are controlled with a stability better than ±0.05 K in a vacuum better than 10 −7   atm . The furnace is also able to work in oxidizing or reducing atmosphere and is mounted on a χ circle table using the φ circle as a driver for precise translation of the sample in the z direction. The sample can be rotated continuously via a mechanical feedthrough. The temperature is measured by means of a thermocouple placed at the sample holder (0.5 mm from the sample position). The temperature has been calibrated up to 1073 K by following the known thermal expansion of an AlCuFe quasicrystal.
doi_str_mv 10.1063/1.1149747
format Article
fullrecord <record><control><sourceid>scitation_cross</sourceid><recordid>TN_cdi_crossref_primary_10_1063_1_1149747</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>rsi</sourcerecordid><originalsourceid>FETCH-LOGICAL-c297t-5aed377dc26adb2ac83dae6aa776f78f572f5d912f4a320d83e7627c086c1bc33</originalsourceid><addsrcrecordid>eNqd0MtKAzEUBuAgCo7VhW-QrUJqLjPJzLIUb1AQRNfhNBcb6VxIMsW-vVNacO_Z_JuPwzk_QreMzhmV4oHNGSsbVaozVDBaN0RJLs5RQakoiVRlfYmuUvqm01SMFeh9gTfha4OzawcXIY_RYT_GDsyUfcShwynkEUNncQ6tI9GlfrtzFv-QCHtsg_cRTA79BPNog0vX6MLDNrmbU87Q59Pjx_KFrN6eX5eLFTG8UZlU4KxQyhouwa45mFpYcBJAKelV7SvFfWUbxn0JglNbCzf9ogytpWFrI8QM3R33mtinFJ3XQwwtxL1mVB_K0Eyfypjs_dEmEzIcrv0f3vXxD-rBevELiehuig</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>A high temperature furnace for in situ and time-resolved x-ray diffraction studies</title><source>AIP Journals Complete</source><source>AIP Digital Archive</source><creator>Capitán, M. J. ; Thouin, N. ; Rostaing, G.</creator><creatorcontrib>Capitán, M. J. ; Thouin, N. ; Rostaing, G.</creatorcontrib><description>A high temperature furnace has been built and mounted on a six-circle goniometer for in situ diffraction studies of polycrystalline and powder samples. Temperatures up to 1400 K are controlled with a stability better than ±0.05 K in a vacuum better than 10 −7   atm . The furnace is also able to work in oxidizing or reducing atmosphere and is mounted on a χ circle table using the φ circle as a driver for precise translation of the sample in the z direction. The sample can be rotated continuously via a mechanical feedthrough. The temperature is measured by means of a thermocouple placed at the sample holder (0.5 mm from the sample position). The temperature has been calibrated up to 1073 K by following the known thermal expansion of an AlCuFe quasicrystal.</description><identifier>ISSN: 0034-6748</identifier><identifier>EISSN: 1089-7623</identifier><identifier>DOI: 10.1063/1.1149747</identifier><identifier>CODEN: RSINAK</identifier><language>eng</language><ispartof>Review of scientific instruments, 1999-05, Vol.70 (5), p.2248-2252</ispartof><rights>American Institute of Physics</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c297t-5aed377dc26adb2ac83dae6aa776f78f572f5d912f4a320d83e7627c086c1bc33</citedby><cites>FETCH-LOGICAL-c297t-5aed377dc26adb2ac83dae6aa776f78f572f5d912f4a320d83e7627c086c1bc33</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://pubs.aip.org/rsi/article-lookup/doi/10.1063/1.1149747$$EHTML$$P50$$Gscitation$$H</linktohtml><link.rule.ids>314,776,780,790,1553,4498,27901,27902,76127,76133</link.rule.ids></links><search><creatorcontrib>Capitán, M. J.</creatorcontrib><creatorcontrib>Thouin, N.</creatorcontrib><creatorcontrib>Rostaing, G.</creatorcontrib><title>A high temperature furnace for in situ and time-resolved x-ray diffraction studies</title><title>Review of scientific instruments</title><description>A high temperature furnace has been built and mounted on a six-circle goniometer for in situ diffraction studies of polycrystalline and powder samples. Temperatures up to 1400 K are controlled with a stability better than ±0.05 K in a vacuum better than 10 −7   atm . The furnace is also able to work in oxidizing or reducing atmosphere and is mounted on a χ circle table using the φ circle as a driver for precise translation of the sample in the z direction. The sample can be rotated continuously via a mechanical feedthrough. The temperature is measured by means of a thermocouple placed at the sample holder (0.5 mm from the sample position). The temperature has been calibrated up to 1073 K by following the known thermal expansion of an AlCuFe quasicrystal.</description><issn>0034-6748</issn><issn>1089-7623</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1999</creationdate><recordtype>article</recordtype><recordid>eNqd0MtKAzEUBuAgCo7VhW-QrUJqLjPJzLIUb1AQRNfhNBcb6VxIMsW-vVNacO_Z_JuPwzk_QreMzhmV4oHNGSsbVaozVDBaN0RJLs5RQakoiVRlfYmuUvqm01SMFeh9gTfha4OzawcXIY_RYT_GDsyUfcShwynkEUNncQ6tI9GlfrtzFv-QCHtsg_cRTA79BPNog0vX6MLDNrmbU87Q59Pjx_KFrN6eX5eLFTG8UZlU4KxQyhouwa45mFpYcBJAKelV7SvFfWUbxn0JglNbCzf9ogytpWFrI8QM3R33mtinFJ3XQwwtxL1mVB_K0Eyfypjs_dEmEzIcrv0f3vXxD-rBevELiehuig</recordid><startdate>19990501</startdate><enddate>19990501</enddate><creator>Capitán, M. J.</creator><creator>Thouin, N.</creator><creator>Rostaing, G.</creator><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>19990501</creationdate><title>A high temperature furnace for in situ and time-resolved x-ray diffraction studies</title><author>Capitán, M. J. ; Thouin, N. ; Rostaing, G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c297t-5aed377dc26adb2ac83dae6aa776f78f572f5d912f4a320d83e7627c086c1bc33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1999</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Capitán, M. J.</creatorcontrib><creatorcontrib>Thouin, N.</creatorcontrib><creatorcontrib>Rostaing, G.</creatorcontrib><collection>CrossRef</collection><jtitle>Review of scientific instruments</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Capitán, M. J.</au><au>Thouin, N.</au><au>Rostaing, G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A high temperature furnace for in situ and time-resolved x-ray diffraction studies</atitle><jtitle>Review of scientific instruments</jtitle><date>1999-05-01</date><risdate>1999</risdate><volume>70</volume><issue>5</issue><spage>2248</spage><epage>2252</epage><pages>2248-2252</pages><issn>0034-6748</issn><eissn>1089-7623</eissn><coden>RSINAK</coden><abstract>A high temperature furnace has been built and mounted on a six-circle goniometer for in situ diffraction studies of polycrystalline and powder samples. Temperatures up to 1400 K are controlled with a stability better than ±0.05 K in a vacuum better than 10 −7   atm . The furnace is also able to work in oxidizing or reducing atmosphere and is mounted on a χ circle table using the φ circle as a driver for precise translation of the sample in the z direction. The sample can be rotated continuously via a mechanical feedthrough. The temperature is measured by means of a thermocouple placed at the sample holder (0.5 mm from the sample position). The temperature has been calibrated up to 1073 K by following the known thermal expansion of an AlCuFe quasicrystal.</abstract><doi>10.1063/1.1149747</doi><tpages>5</tpages></addata></record>
fulltext fulltext
identifier ISSN: 0034-6748
ispartof Review of scientific instruments, 1999-05, Vol.70 (5), p.2248-2252
issn 0034-6748
1089-7623
language eng
recordid cdi_crossref_primary_10_1063_1_1149747
source AIP Journals Complete; AIP Digital Archive
title A high temperature furnace for in situ and time-resolved x-ray diffraction studies
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-02T19%3A33%3A12IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-scitation_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=A%20high%20temperature%20furnace%20for%20in%20situ%20and%20time-resolved%20x-ray%20diffraction%20studies&rft.jtitle=Review%20of%20scientific%20instruments&rft.au=Capit%C3%A1n,%20M.%20J.&rft.date=1999-05-01&rft.volume=70&rft.issue=5&rft.spage=2248&rft.epage=2252&rft.pages=2248-2252&rft.issn=0034-6748&rft.eissn=1089-7623&rft.coden=RSINAK&rft_id=info:doi/10.1063/1.1149747&rft_dat=%3Cscitation_cross%3Ersi%3C/scitation_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true