Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers
We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a 141 μm×141 μm Nb-Al-Al 2 O 3 -Al-Nb superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy reso...
Gespeichert in:
Veröffentlicht in: | Review of Scientific Instruments 1998-01, Vol.69 (1), p.25-31 |
---|---|
Hauptverfasser: | , , , , , , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | 31 |
---|---|
container_issue | 1 |
container_start_page | 25 |
container_title | Review of Scientific Instruments |
container_volume | 69 |
creator | Frank, M. Hiller, L. J. le Grand, J. B. Mears, C. A. Labov, S. E. Lindeman, M. A. Netel, H. Chow, D. Barfknecht, A.T. |
description | We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a
141 μm×141 μm
Nb-Al-Al
2
O
3
-Al-Nb
superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy resolution of this energy-dispersive spectrometer for soft x rays with energies between 70 and 700 eV and investigated its performance at count rates up to nearly 60 000 cps. At count rates of several 100 cps we achieved an energy resolution of 5.9 eV (FWHM) and an electronic noise of 4.5 eV for 277 eV x rays (the energy corresponding to C
K
). Increasing the count rate, the resolution 277 eV remained below 10 eV for count rates up to
∼10 000
cps
and then degraded to 13 eV at 23 000 cps and 20 eV at 50 000 cps. These results were achieved using a commercially available spectroscopy amplifier with a baseline restorer. No pile-up rejection was applied in these measurements. Our results show that STJ detectors can operate at count rates approaching those of semiconductor detectors while still providing a significantly better energy resolution for soft x rays. Thus STJ detectors may prove very useful in microanalysis, synchrotron x-ray fluorescence (XRF) applications, and XRF analysis of light elements (
K
lines) and transition elements (
L
lines). |
doi_str_mv | 10.1063/1.1148474 |
format | Article |
fullrecord | <record><control><sourceid>scitation_cross</sourceid><recordid>TN_cdi_crossref_primary_10_1063_1_1148474</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>rsi</sourcerecordid><originalsourceid>FETCH-LOGICAL-c321t-9162de47f225b41fbb583c43f87ef8b631e576b2b4f519876237197c9901a1bb3</originalsourceid><addsrcrecordid>eNqdkF9LwzAUxYMoOKcPfoP4qNCZ26RN-yhj_oGBL_ockjRZO7akJKm4b2_rBr57Xw5cfhzOOQjdAlkAKekjLABYxTg7QzMgVZ3xMqfnaEYIZVnJWXWJrmLckvEKgBlqV86EzQEHE_1uSJ13WLoGt92mxdoPLuEgk8G9CdaHvXTaYG9xHMaH9q4ZdOrcBqfBObPD28HpX4vvLMgDjr3RKfi9SSbEa3Rh5S6am5PO0efz6mP5mq3fX96WT-tM0xxSVkOZN4Zxm-eFYmCVKiqqGbUVN7ZSJQVT8FLlitkC6mpqx6Hmuq4JSFCKztHd0dfH1Imou2R0O0Z1YxZRlCVU-cjcHxkdfIzBWNGHbi_DQQAR04wCxGnGkX04spOVnNr9D_7y4Q8UfWPpD2tVgkc</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers</title><source>AIP Digital Archive</source><creator>Frank, M. ; Hiller, L. J. ; le Grand, J. B. ; Mears, C. A. ; Labov, S. E. ; Lindeman, M. A. ; Netel, H. ; Chow, D. ; Barfknecht, A.T.</creator><creatorcontrib>Frank, M. ; Hiller, L. J. ; le Grand, J. B. ; Mears, C. A. ; Labov, S. E. ; Lindeman, M. A. ; Netel, H. ; Chow, D. ; Barfknecht, A.T.</creatorcontrib><description>We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a
141 μm×141 μm
Nb-Al-Al
2
O
3
-Al-Nb
superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy resolution of this energy-dispersive spectrometer for soft x rays with energies between 70 and 700 eV and investigated its performance at count rates up to nearly 60 000 cps. At count rates of several 100 cps we achieved an energy resolution of 5.9 eV (FWHM) and an electronic noise of 4.5 eV for 277 eV x rays (the energy corresponding to C
K
). Increasing the count rate, the resolution 277 eV remained below 10 eV for count rates up to
∼10 000
cps
and then degraded to 13 eV at 23 000 cps and 20 eV at 50 000 cps. These results were achieved using a commercially available spectroscopy amplifier with a baseline restorer. No pile-up rejection was applied in these measurements. Our results show that STJ detectors can operate at count rates approaching those of semiconductor detectors while still providing a significantly better energy resolution for soft x rays. Thus STJ detectors may prove very useful in microanalysis, synchrotron x-ray fluorescence (XRF) applications, and XRF analysis of light elements (
K
lines) and transition elements (
L
lines).</description><identifier>ISSN: 0034-6748</identifier><identifier>EISSN: 1089-7623</identifier><identifier>DOI: 10.1063/1.1148474</identifier><identifier>CODEN: RSINAK</identifier><language>eng</language><publisher>United States</publisher><subject>ALUMINIUM ; ALUMINIUM OXIDES ; ENERGY RESOLUTION ; EV RANGE 10-100 ; EV RANGE 100-1000 ; FABRICATION ; FLUORESCENCE ; INSTRUMENTATION, INCLUDING NUCLEAR AND PARTICLE DETECTORS ; NIOBIUM ; SUPERCONDUCTING JUNCTIONS ; SYNCHROTRON RADIATION ; TUNNEL EFFECT ; USES ; X-RAY DETECTION ; X-RAY FLUORESCENCE ANALYSIS ; X-RAY SPECTROMETERS</subject><ispartof>Review of Scientific Instruments, 1998-01, Vol.69 (1), p.25-31</ispartof><rights>American Institute of Physics</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c321t-9162de47f225b41fbb583c43f87ef8b631e576b2b4f519876237197c9901a1bb3</citedby><cites>FETCH-LOGICAL-c321t-9162de47f225b41fbb583c43f87ef8b631e576b2b4f519876237197c9901a1bb3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://pubs.aip.org/rsi/article-lookup/doi/10.1063/1.1148474$$EHTML$$P50$$Gscitation$$H</linktohtml><link.rule.ids>314,776,780,881,1553,27901,27902,76132</link.rule.ids><backlink>$$Uhttps://www.osti.gov/biblio/566182$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Frank, M.</creatorcontrib><creatorcontrib>Hiller, L. J.</creatorcontrib><creatorcontrib>le Grand, J. B.</creatorcontrib><creatorcontrib>Mears, C. A.</creatorcontrib><creatorcontrib>Labov, S. E.</creatorcontrib><creatorcontrib>Lindeman, M. A.</creatorcontrib><creatorcontrib>Netel, H.</creatorcontrib><creatorcontrib>Chow, D.</creatorcontrib><creatorcontrib>Barfknecht, A.T.</creatorcontrib><title>Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers</title><title>Review of Scientific Instruments</title><description>We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a
141 μm×141 μm
Nb-Al-Al
2
O
3
-Al-Nb
superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy resolution of this energy-dispersive spectrometer for soft x rays with energies between 70 and 700 eV and investigated its performance at count rates up to nearly 60 000 cps. At count rates of several 100 cps we achieved an energy resolution of 5.9 eV (FWHM) and an electronic noise of 4.5 eV for 277 eV x rays (the energy corresponding to C
K
). Increasing the count rate, the resolution 277 eV remained below 10 eV for count rates up to
∼10 000
cps
and then degraded to 13 eV at 23 000 cps and 20 eV at 50 000 cps. These results were achieved using a commercially available spectroscopy amplifier with a baseline restorer. No pile-up rejection was applied in these measurements. Our results show that STJ detectors can operate at count rates approaching those of semiconductor detectors while still providing a significantly better energy resolution for soft x rays. Thus STJ detectors may prove very useful in microanalysis, synchrotron x-ray fluorescence (XRF) applications, and XRF analysis of light elements (
K
lines) and transition elements (
L
lines).</description><subject>ALUMINIUM</subject><subject>ALUMINIUM OXIDES</subject><subject>ENERGY RESOLUTION</subject><subject>EV RANGE 10-100</subject><subject>EV RANGE 100-1000</subject><subject>FABRICATION</subject><subject>FLUORESCENCE</subject><subject>INSTRUMENTATION, INCLUDING NUCLEAR AND PARTICLE DETECTORS</subject><subject>NIOBIUM</subject><subject>SUPERCONDUCTING JUNCTIONS</subject><subject>SYNCHROTRON RADIATION</subject><subject>TUNNEL EFFECT</subject><subject>USES</subject><subject>X-RAY DETECTION</subject><subject>X-RAY FLUORESCENCE ANALYSIS</subject><subject>X-RAY SPECTROMETERS</subject><issn>0034-6748</issn><issn>1089-7623</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1998</creationdate><recordtype>article</recordtype><recordid>eNqdkF9LwzAUxYMoOKcPfoP4qNCZ26RN-yhj_oGBL_ockjRZO7akJKm4b2_rBr57Xw5cfhzOOQjdAlkAKekjLABYxTg7QzMgVZ3xMqfnaEYIZVnJWXWJrmLckvEKgBlqV86EzQEHE_1uSJ13WLoGt92mxdoPLuEgk8G9CdaHvXTaYG9xHMaH9q4ZdOrcBqfBObPD28HpX4vvLMgDjr3RKfi9SSbEa3Rh5S6am5PO0efz6mP5mq3fX96WT-tM0xxSVkOZN4Zxm-eFYmCVKiqqGbUVN7ZSJQVT8FLlitkC6mpqx6Hmuq4JSFCKztHd0dfH1Imou2R0O0Z1YxZRlCVU-cjcHxkdfIzBWNGHbi_DQQAR04wCxGnGkX04spOVnNr9D_7y4Q8UfWPpD2tVgkc</recordid><startdate>199801</startdate><enddate>199801</enddate><creator>Frank, M.</creator><creator>Hiller, L. J.</creator><creator>le Grand, J. B.</creator><creator>Mears, C. A.</creator><creator>Labov, S. E.</creator><creator>Lindeman, M. A.</creator><creator>Netel, H.</creator><creator>Chow, D.</creator><creator>Barfknecht, A.T.</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>199801</creationdate><title>Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers</title><author>Frank, M. ; Hiller, L. J. ; le Grand, J. B. ; Mears, C. A. ; Labov, S. E. ; Lindeman, M. A. ; Netel, H. ; Chow, D. ; Barfknecht, A.T.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c321t-9162de47f225b41fbb583c43f87ef8b631e576b2b4f519876237197c9901a1bb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1998</creationdate><topic>ALUMINIUM</topic><topic>ALUMINIUM OXIDES</topic><topic>ENERGY RESOLUTION</topic><topic>EV RANGE 10-100</topic><topic>EV RANGE 100-1000</topic><topic>FABRICATION</topic><topic>FLUORESCENCE</topic><topic>INSTRUMENTATION, INCLUDING NUCLEAR AND PARTICLE DETECTORS</topic><topic>NIOBIUM</topic><topic>SUPERCONDUCTING JUNCTIONS</topic><topic>SYNCHROTRON RADIATION</topic><topic>TUNNEL EFFECT</topic><topic>USES</topic><topic>X-RAY DETECTION</topic><topic>X-RAY FLUORESCENCE ANALYSIS</topic><topic>X-RAY SPECTROMETERS</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Frank, M.</creatorcontrib><creatorcontrib>Hiller, L. J.</creatorcontrib><creatorcontrib>le Grand, J. B.</creatorcontrib><creatorcontrib>Mears, C. A.</creatorcontrib><creatorcontrib>Labov, S. E.</creatorcontrib><creatorcontrib>Lindeman, M. A.</creatorcontrib><creatorcontrib>Netel, H.</creatorcontrib><creatorcontrib>Chow, D.</creatorcontrib><creatorcontrib>Barfknecht, A.T.</creatorcontrib><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Review of Scientific Instruments</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Frank, M.</au><au>Hiller, L. J.</au><au>le Grand, J. B.</au><au>Mears, C. A.</au><au>Labov, S. E.</au><au>Lindeman, M. A.</au><au>Netel, H.</au><au>Chow, D.</au><au>Barfknecht, A.T.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers</atitle><jtitle>Review of Scientific Instruments</jtitle><date>1998-01</date><risdate>1998</risdate><volume>69</volume><issue>1</issue><spage>25</spage><epage>31</epage><pages>25-31</pages><issn>0034-6748</issn><eissn>1089-7623</eissn><coden>RSINAK</coden><abstract>We present experimental results obtained with a cryogenically cooled, high-resolution x-ray spectrometer based on a
141 μm×141 μm
Nb-Al-Al
2
O
3
-Al-Nb
superconducting tunnel junction (STJ) detector in a demonstration experiment. Using monochromatized synchrotron radiation we studied the energy resolution of this energy-dispersive spectrometer for soft x rays with energies between 70 and 700 eV and investigated its performance at count rates up to nearly 60 000 cps. At count rates of several 100 cps we achieved an energy resolution of 5.9 eV (FWHM) and an electronic noise of 4.5 eV for 277 eV x rays (the energy corresponding to C
K
). Increasing the count rate, the resolution 277 eV remained below 10 eV for count rates up to
∼10 000
cps
and then degraded to 13 eV at 23 000 cps and 20 eV at 50 000 cps. These results were achieved using a commercially available spectroscopy amplifier with a baseline restorer. No pile-up rejection was applied in these measurements. Our results show that STJ detectors can operate at count rates approaching those of semiconductor detectors while still providing a significantly better energy resolution for soft x rays. Thus STJ detectors may prove very useful in microanalysis, synchrotron x-ray fluorescence (XRF) applications, and XRF analysis of light elements (
K
lines) and transition elements (
L
lines).</abstract><cop>United States</cop><doi>10.1063/1.1148474</doi><tpages>7</tpages></addata></record> |
fulltext | fulltext |
identifier | ISSN: 0034-6748 |
ispartof | Review of Scientific Instruments, 1998-01, Vol.69 (1), p.25-31 |
issn | 0034-6748 1089-7623 |
language | eng |
recordid | cdi_crossref_primary_10_1063_1_1148474 |
source | AIP Digital Archive |
subjects | ALUMINIUM ALUMINIUM OXIDES ENERGY RESOLUTION EV RANGE 10-100 EV RANGE 100-1000 FABRICATION FLUORESCENCE INSTRUMENTATION, INCLUDING NUCLEAR AND PARTICLE DETECTORS NIOBIUM SUPERCONDUCTING JUNCTIONS SYNCHROTRON RADIATION TUNNEL EFFECT USES X-RAY DETECTION X-RAY FLUORESCENCE ANALYSIS X-RAY SPECTROMETERS |
title | Energy resolution and high count rate performance of superconducting tunnel junction x-ray spectrometers |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-02-08T07%3A33%3A48IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-scitation_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Energy%20resolution%20and%20high%20count%20rate%20performance%20of%20superconducting%20tunnel%20junction%20x-ray%20spectrometers&rft.jtitle=Review%20of%20Scientific%20Instruments&rft.au=Frank,%20M.&rft.date=1998-01&rft.volume=69&rft.issue=1&rft.spage=25&rft.epage=31&rft.pages=25-31&rft.issn=0034-6748&rft.eissn=1089-7623&rft.coden=RSINAK&rft_id=info:doi/10.1063/1.1148474&rft_dat=%3Cscitation_cross%3Ersi%3C/scitation_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |