Solvothermal synthesis and electrochemical properties of 3D flower-like iron phthalocyanine hierarchical nanostructure
In the present work, a highly uniform three-dimensional flower-like 2,9,16,23-tetra-nitrophthalocyanine iron (TNFePc) hierarchical nanostructure has been successfully obtained by a facile ethylene glycol solvothermal synthetic route. The as-obtained product was characterized by mass spectroscopy, fi...
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| Veröffentlicht in: | Nanoscale 2011-01, Vol.3 (12), p.5126-5131 |
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| creator | Mu, Jingbo Shao, Changlu Guo, Zengcai Zhang, Mingyi Zhang, Zhenyi Zhang, Peng Chen, Bin Liu, Yichun |
| description | In the present work, a highly uniform three-dimensional flower-like 2,9,16,23-tetra-nitrophthalocyanine iron (TNFePc) hierarchical nanostructure has been successfully obtained by a facile ethylene glycol solvothermal synthetic route. The as-obtained product was characterized by mass spectroscopy, field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), IR spectroscopy, UV-vis spectroscopy, and Brunauer-Emmett-Teller analysis. The results showed that the flower-like hierarchical nanostructure was made up of numerous two-dimensional nanoplates with a thickness of about 50 nm. Electrochemical measurements revealed that the TNFePc hierarchical nanostructure exhibited excellent capacitance behavior, which could be ascribed to the ultrahigh surface area and large pore volume. Finally, a possible mechanism for the formation of three-dimensional flower-like TNFePc was suggested.
A three-dimensional flower-like TNFePc hierarchical nanostructure is successfully fabricated by a facile solvothermal synthetic route, and shows high capacitive behavior as an electrode material for supercapacitors. |
| doi_str_mv | 10.1039/c1nr10627a |
| format | Article |
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A three-dimensional flower-like TNFePc hierarchical nanostructure is successfully fabricated by a facile solvothermal synthetic route, and shows high capacitive behavior as an electrode material for supercapacitors.</description><identifier>ISSN: 2040-3364</identifier><identifier>EISSN: 2040-3372</identifier><identifier>DOI: 10.1039/c1nr10627a</identifier><language>eng</language><subject>Iron ; Mass spectroscopy ; Nanocomposites ; Nanomaterials ; Nanostructure ; Scanning electron microscopy ; Spectroscopy ; Three dimensional</subject><ispartof>Nanoscale, 2011-01, Vol.3 (12), p.5126-5131</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c378t-5ae06b71a8a522ea428f5ccbaa70c44dc68e57e5f19b500cede89e118a58bf023</citedby><cites>FETCH-LOGICAL-c378t-5ae06b71a8a522ea428f5ccbaa70c44dc68e57e5f19b500cede89e118a58bf023</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,778,782,27911,27912</link.rule.ids></links><search><creatorcontrib>Mu, Jingbo</creatorcontrib><creatorcontrib>Shao, Changlu</creatorcontrib><creatorcontrib>Guo, Zengcai</creatorcontrib><creatorcontrib>Zhang, Mingyi</creatorcontrib><creatorcontrib>Zhang, Zhenyi</creatorcontrib><creatorcontrib>Zhang, Peng</creatorcontrib><creatorcontrib>Chen, Bin</creatorcontrib><creatorcontrib>Liu, Yichun</creatorcontrib><title>Solvothermal synthesis and electrochemical properties of 3D flower-like iron phthalocyanine hierarchical nanostructure</title><title>Nanoscale</title><description>In the present work, a highly uniform three-dimensional flower-like 2,9,16,23-tetra-nitrophthalocyanine iron (TNFePc) hierarchical nanostructure has been successfully obtained by a facile ethylene glycol solvothermal synthetic route. The as-obtained product was characterized by mass spectroscopy, field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), IR spectroscopy, UV-vis spectroscopy, and Brunauer-Emmett-Teller analysis. The results showed that the flower-like hierarchical nanostructure was made up of numerous two-dimensional nanoplates with a thickness of about 50 nm. Electrochemical measurements revealed that the TNFePc hierarchical nanostructure exhibited excellent capacitance behavior, which could be ascribed to the ultrahigh surface area and large pore volume. Finally, a possible mechanism for the formation of three-dimensional flower-like TNFePc was suggested.
A three-dimensional flower-like TNFePc hierarchical nanostructure is successfully fabricated by a facile solvothermal synthetic route, and shows high capacitive behavior as an electrode material for supercapacitors.</description><subject>Iron</subject><subject>Mass spectroscopy</subject><subject>Nanocomposites</subject><subject>Nanomaterials</subject><subject>Nanostructure</subject><subject>Scanning electron microscopy</subject><subject>Spectroscopy</subject><subject>Three dimensional</subject><issn>2040-3364</issn><issn>2040-3372</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNp9kE1LxDAQhoMouK5evAvxJkI1adomPcr6CQse1HNJ0wmNpklN2pX991ZXVrx4mheeZ4bhReiYkgtKWHmpqAuUFCmXO2iWkowkjPF0d5uLbB8dxPhKSFGygs3Q6snblR9aCJ20OK7dFKOJWLoGgwU1BK9a6IyaaB98D2EwELHXmF1jbf0HhMSaN8AmeIf7dmil9WotnXGAWwNBBtV-bzvpfBzCqIYxwCHa09JGOPqZc_Rye_O8uE-Wj3cPi6tlohgXQ5JLIEXNqRQyT1OQWSp0rlQtJScqyxpVCMg55JqWdU6IggZECZROuqg1SdkcnW3uTr-_jxCHqjNRgbXSgR9jRQklgvOUiUk936gq-BgD6KoPppNhPUnVV7nVb7mTfLKRQ1Rb7w8__Y9XfaPZJwk2hks</recordid><startdate>20110101</startdate><enddate>20110101</enddate><creator>Mu, Jingbo</creator><creator>Shao, Changlu</creator><creator>Guo, Zengcai</creator><creator>Zhang, Mingyi</creator><creator>Zhang, Zhenyi</creator><creator>Zhang, Peng</creator><creator>Chen, Bin</creator><creator>Liu, Yichun</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20110101</creationdate><title>Solvothermal synthesis and electrochemical properties of 3D flower-like iron phthalocyanine hierarchical nanostructure</title><author>Mu, Jingbo ; Shao, Changlu ; Guo, Zengcai ; Zhang, Mingyi ; Zhang, Zhenyi ; Zhang, Peng ; Chen, Bin ; Liu, Yichun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c378t-5ae06b71a8a522ea428f5ccbaa70c44dc68e57e5f19b500cede89e118a58bf023</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Iron</topic><topic>Mass spectroscopy</topic><topic>Nanocomposites</topic><topic>Nanomaterials</topic><topic>Nanostructure</topic><topic>Scanning electron microscopy</topic><topic>Spectroscopy</topic><topic>Three dimensional</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Mu, Jingbo</creatorcontrib><creatorcontrib>Shao, Changlu</creatorcontrib><creatorcontrib>Guo, Zengcai</creatorcontrib><creatorcontrib>Zhang, Mingyi</creatorcontrib><creatorcontrib>Zhang, Zhenyi</creatorcontrib><creatorcontrib>Zhang, Peng</creatorcontrib><creatorcontrib>Chen, Bin</creatorcontrib><creatorcontrib>Liu, Yichun</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Nanoscale</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mu, Jingbo</au><au>Shao, Changlu</au><au>Guo, Zengcai</au><au>Zhang, Mingyi</au><au>Zhang, Zhenyi</au><au>Zhang, Peng</au><au>Chen, Bin</au><au>Liu, Yichun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Solvothermal synthesis and electrochemical properties of 3D flower-like iron phthalocyanine hierarchical nanostructure</atitle><jtitle>Nanoscale</jtitle><date>2011-01-01</date><risdate>2011</risdate><volume>3</volume><issue>12</issue><spage>5126</spage><epage>5131</epage><pages>5126-5131</pages><issn>2040-3364</issn><eissn>2040-3372</eissn><abstract>In the present work, a highly uniform three-dimensional flower-like 2,9,16,23-tetra-nitrophthalocyanine iron (TNFePc) hierarchical nanostructure has been successfully obtained by a facile ethylene glycol solvothermal synthetic route. The as-obtained product was characterized by mass spectroscopy, field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM), IR spectroscopy, UV-vis spectroscopy, and Brunauer-Emmett-Teller analysis. The results showed that the flower-like hierarchical nanostructure was made up of numerous two-dimensional nanoplates with a thickness of about 50 nm. Electrochemical measurements revealed that the TNFePc hierarchical nanostructure exhibited excellent capacitance behavior, which could be ascribed to the ultrahigh surface area and large pore volume. Finally, a possible mechanism for the formation of three-dimensional flower-like TNFePc was suggested.
A three-dimensional flower-like TNFePc hierarchical nanostructure is successfully fabricated by a facile solvothermal synthetic route, and shows high capacitive behavior as an electrode material for supercapacitors.</abstract><doi>10.1039/c1nr10627a</doi><tpages>6</tpages></addata></record> |
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| ispartof | Nanoscale, 2011-01, Vol.3 (12), p.5126-5131 |
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| language | eng |
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| source | Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
| subjects | Iron Mass spectroscopy Nanocomposites Nanomaterials Nanostructure Scanning electron microscopy Spectroscopy Three dimensional |
| title | Solvothermal synthesis and electrochemical properties of 3D flower-like iron phthalocyanine hierarchical nanostructure |
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