Simultaneous precipitation and discharge plasma processing for one-step synthesis of α-Fe 2 O 3 -Fe 3 O 4 /graphene visible light magnetically separable photocatalysts

A novel facile combination of precipitation and plasma discharge reaction is successfully employed for one-step synthesis of an α-Fe O -Fe O graphene nanocomposite (GFs). The co-existence and anchoring of hematite (α-Fe O ) and magnetite (Fe O ) nanoparticles onto a graphene sheet in the as synthesi...

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Veröffentlicht in:RSC advances 2023-03, Vol.13 (11), p.7372-7379
Hauptverfasser: Tuyen, Nguyen Long, Toan, Tran Quoc, Hung, Nguyen Ba, Trieu, Pham Quoc, Dinh, Nguyen Ngoc, Do, Danh Bich, Van Thanh, Dang, Nguyen, Van-Truong
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container_end_page 7379
container_issue 11
container_start_page 7372
container_title RSC advances
container_volume 13
creator Tuyen, Nguyen Long
Toan, Tran Quoc
Hung, Nguyen Ba
Trieu, Pham Quoc
Dinh, Nguyen Ngoc
Do, Danh Bich
Van Thanh, Dang
Nguyen, Van-Truong
description A novel facile combination of precipitation and plasma discharge reaction is successfully employed for one-step synthesis of an α-Fe O -Fe O graphene nanocomposite (GFs). The co-existence and anchoring of hematite (α-Fe O ) and magnetite (Fe O ) nanoparticles onto a graphene sheet in the as synthesized GFs were verified by results of XRD, Raman, SEM, TEM, and XPS. HRTEM characterization was used for confirming the bonding between α-Fe O /Fe O nanoparticles and the graphene sheet. Consequently, GFs shows superior photodegrading performance towards methylene blue (MB), compared to individual α-Fe O /Fe O nanoparticles, as a result of band gap narrowing and the electron-hole pair recombination rate reducing. Moreover, GFs allows a good possibility of separating and recycling under an external-magnetic field, suggesting potential in visible-light-promoted photocatalytic applications.
doi_str_mv 10.1039/D2RA06844C
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title Simultaneous precipitation and discharge plasma processing for one-step synthesis of α-Fe 2 O 3 -Fe 3 O 4 /graphene visible light magnetically separable photocatalysts
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