Morphology-controlled synthesis of MoS 2 using citric acid as a complexing agent and self-assembly inducer for high electrochemical performance

Two-dimensional MoS with a controllable morphology was prepared a simple one-step hydrothermal method. Citric acid was used as a complexing agent and self-assembly inducer. The morphology of MoS changed from clusters to nanosheets, and, eventually, to stacked nanorods. A formation mechanism is propo...

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Veröffentlicht in:RSC advances 2022-10, Vol.12 (44), p.28463-28472
Hauptverfasser: Bai, Mingmin, Li, Weixin, Yang, Hu, Dong, Weixia, Wang, Qinyu, Chang, Qibing
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container_end_page 28472
container_issue 44
container_start_page 28463
container_title RSC advances
container_volume 12
creator Bai, Mingmin
Li, Weixin
Yang, Hu
Dong, Weixia
Wang, Qinyu
Chang, Qibing
description Two-dimensional MoS with a controllable morphology was prepared a simple one-step hydrothermal method. Citric acid was used as a complexing agent and self-assembly inducer. The morphology of MoS changed from clusters to nanosheets, and, eventually, to stacked nanorods. A formation mechanism is proposed for the observed evolution of the morphology. The nanosheet structure presents a relatively large specific surface area, more exposed active sites and greater 1T phase content compared to the other morphologies. The electrochemical performance tests show that the MoS nanosheets exhibit excellent electrochemical behavior. Their specific capacitance is 320.5 F g , and their capacitance retention is up to 95% after 5000 cycles at 5 mA cm . This work provides a feasible approach for changing the morphology of MoS for high efficiency electrode materials for supercapacitors.
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title Morphology-controlled synthesis of MoS 2 using citric acid as a complexing agent and self-assembly inducer for high electrochemical performance
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