Synthesis and NMR analysis of 13 C and 15 N-labeled long-chain polyamines (LCPAs)

15 N, 13 C, or both isotope labels were introduced in selected positions of several LCPAs containing 5, 11, or 13 nitrogens. The number of transformations during chemical synthesis was minimized by coupling Fmoc-glycine- 15 N, Fmoc-glycine-1- 13 C, or Fmoc-β-alanine simultaneously at both ends of th...

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Veröffentlicht in:RSC advances 2016, Vol.6 (96), p.93343-93348
Hauptverfasser: Abacilar, Maryna, Daus, Fabian, Haas, Christian, Brückner, Stephan Ingmar, Brunner, Eike, Geyer, Armin
Format: Artikel
Sprache:eng
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