Template-free synthesis of TiO 2 microspheres with tunable particle size via a non-aqueous sol–gel process

TiO 2 microspheres with tunable particle size were prepared in alcohols without a template via a facile non-aqueous sol–gel process, on the basis of an ester elimination mechanism. The diameter of TiO 2 microspheres in the range of 0.4–2.9 μm was controlled by the ratio of methanol in the solvent....

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Veröffentlicht in:CrystEngComm 2014, Vol.16 (34), p.7881-7884
Hauptverfasser: He, Kay, Zhao, Gaoling, Han, Gaorong
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description TiO 2 microspheres with tunable particle size were prepared in alcohols without a template via a facile non-aqueous sol–gel process, on the basis of an ester elimination mechanism. The diameter of TiO 2 microspheres in the range of 0.4–2.9 μm was controlled by the ratio of methanol in the solvent.
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title Template-free synthesis of TiO 2 microspheres with tunable particle size via a non-aqueous sol–gel process
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