Continuous Organic Synthesis in a Spinning Tube-in-Tube Reactor: TEMPO-Catalyzed Oxidation of Alcohols by Hypochlorite

Continuous production of aldehydes in high yields (≥90%) can be accomplished by feeding aqueous (sodium hypochlorite/sodium bicarbonate, pH 8.5) and organic (TEMPO/tetrabutylammonium bromide/primary alcohol/toluene or CH2Cl2) solutions through the inlets of a spinning tube-in-tube reactor (STT react...

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Veröffentlicht in:	Organic process research & development 2008-09, Vol.12 (5), p.946-949
Hauptverfasser:	Hampton, Philip D, Whealon, Matthew D, Roberts, Lisa M, Yaeger, Andrew A, Boydson, Rick
Format:	Artikel
Sprache:	eng
Online-Zugang:	Volltext
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