Process Safety Evaluation To Identify the Inherent Hazards of a Highly Exothermic Ritter Reaction Using Adiabatic and Isothermal Calorimeters

This paper describes the process safety studies that were carried out prior to the scale-up for the initial process containing the reaction of 1,3-dimethyladamantane with sulfuric acid and acetonitrile. The reaction temperature is set at 13 °C followed by heating to 23 °C for progress of the reactio...

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Veröffentlicht in:	Organic process research & development 2013-12, Vol.17 (12), p.1597-1602
Hauptverfasser:	Veedhi, Srinivasarao, Babu, Subramani Ramesh
Format:	Artikel
Sprache:	eng
Online-Zugang:	Volltext
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