Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas
The nitrogen adsorption isotherm measured at 77 K in the relative pressure range from about 5 × 10-7 to 0.988 for a macroporous silica is reported in a tabular form. The isotherm data are in good agreement in the high-pressure range with the reference data published by Gregg and Sing and by Kiselev...
Gespeichert in:
| Veröffentlicht in: | Langmuir 1999-08, Vol.15 (16), p.5410-5413 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 5413 |
|---|---|
| container_issue | 16 |
| container_start_page | 5410 |
| container_title | Langmuir |
| container_volume | 15 |
| creator | Jaroniec, Mietek Kruk, Michal Olivier, James P |
| description | The nitrogen adsorption isotherm measured at 77 K in the relative pressure range from about 5 × 10-7 to 0.988 for a macroporous silica is reported in a tabular form. The isotherm data are in good agreement in the high-pressure range with the reference data published by Gregg and Sing and by Kiselev and Aristov and provide an extension of the latter data to the low-pressure region, for which a reliable reference isotherm was not availalable in the literature. Application of the currently reported reference adsorption isotherm is discussed. The data can be used in comparative analysis (αs-plot or t-plot) to evaluate the external surface area, micropore volume, primary mesopore volume, and total surface area as well as to analyze surface properties of silica-based materials. The adsorption isotherm can also be applied as a statistical film thickness curve in the calculation of the mesopore size distribution. |
| doi_str_mv | 10.1021/la990136e |
| format | Article |
| fullrecord | <record><control><sourceid>acs_cross</sourceid><recordid>TN_cdi_crossref_primary_10_1021_la990136e</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>c225997204</sourcerecordid><originalsourceid>FETCH-LOGICAL-a324t-338800999a13f27463e812776844e656d44c4f226184abb8b176a82a1c81fab43</originalsourceid><addsrcrecordid>eNptkDtPw0AQhE8IJEKg4B-4gILCcC_fo4wCCUgRDyXUp_XZBw7GZ905EvDrcTAKDdUW8-3OziB0SvAlwZRc1aA1JkyUe2hEMorTTFG5j0ZYcpZKLtghOopxjTHWjOsRWiw7aAoIRXJfdcG_lE0yKaIPbVf5JrmGDhLnQzJ9hQC2K0P1BT-Kd8k9NL71wW9isqzqykI8RgcO6lie_M4xep7drKa36eJhfjedLFJglHcpY0r1_loDYY5unyoVoVIKxXkpMlFwbrmjVBDFIc9VTqQARYFYRRzknI3RxXDXBh9jKJ1pQ_UO4dMQbLY1mF0NPXs2sC1EC7UL0Ngq_i1orIRgPZYOWBW78mMnQ3gzQjKZmdXj0ujZfIWJouap588HHmw0a78JTR_4H_tvBnV2gA</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas</title><source>American Chemical Society Journals</source><creator>Jaroniec, Mietek ; Kruk, Michal ; Olivier, James P</creator><creatorcontrib>Jaroniec, Mietek ; Kruk, Michal ; Olivier, James P</creatorcontrib><description>The nitrogen adsorption isotherm measured at 77 K in the relative pressure range from about 5 × 10-7 to 0.988 for a macroporous silica is reported in a tabular form. The isotherm data are in good agreement in the high-pressure range with the reference data published by Gregg and Sing and by Kiselev and Aristov and provide an extension of the latter data to the low-pressure region, for which a reliable reference isotherm was not availalable in the literature. Application of the currently reported reference adsorption isotherm is discussed. The data can be used in comparative analysis (αs-plot or t-plot) to evaluate the external surface area, micropore volume, primary mesopore volume, and total surface area as well as to analyze surface properties of silica-based materials. The adsorption isotherm can also be applied as a statistical film thickness curve in the calculation of the mesopore size distribution.</description><identifier>ISSN: 0743-7463</identifier><identifier>EISSN: 1520-5827</identifier><identifier>DOI: 10.1021/la990136e</identifier><identifier>CODEN: LANGD5</identifier><language>eng</language><publisher>Washington, DC: American Chemical Society</publisher><subject>Chemistry ; Colloidal state and disperse state ; Exact sciences and technology ; General and physical chemistry ; Porous materials</subject><ispartof>Langmuir, 1999-08, Vol.15 (16), p.5410-5413</ispartof><rights>Copyright © 1999 American Chemical Society</rights><rights>1999 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a324t-338800999a13f27463e812776844e656d44c4f226184abb8b176a82a1c81fab43</citedby><cites>FETCH-LOGICAL-a324t-338800999a13f27463e812776844e656d44c4f226184abb8b176a82a1c81fab43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://pubs.acs.org/doi/pdf/10.1021/la990136e$$EPDF$$P50$$Gacs$$H</linktopdf><linktohtml>$$Uhttps://pubs.acs.org/doi/10.1021/la990136e$$EHTML$$P50$$Gacs$$H</linktohtml><link.rule.ids>314,780,784,2765,27076,27924,27925,56738,56788</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=1908663$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Jaroniec, Mietek</creatorcontrib><creatorcontrib>Kruk, Michal</creatorcontrib><creatorcontrib>Olivier, James P</creatorcontrib><title>Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas</title><title>Langmuir</title><addtitle>Langmuir</addtitle><description>The nitrogen adsorption isotherm measured at 77 K in the relative pressure range from about 5 × 10-7 to 0.988 for a macroporous silica is reported in a tabular form. The isotherm data are in good agreement in the high-pressure range with the reference data published by Gregg and Sing and by Kiselev and Aristov and provide an extension of the latter data to the low-pressure region, for which a reliable reference isotherm was not availalable in the literature. Application of the currently reported reference adsorption isotherm is discussed. The data can be used in comparative analysis (αs-plot or t-plot) to evaluate the external surface area, micropore volume, primary mesopore volume, and total surface area as well as to analyze surface properties of silica-based materials. The adsorption isotherm can also be applied as a statistical film thickness curve in the calculation of the mesopore size distribution.</description><subject>Chemistry</subject><subject>Colloidal state and disperse state</subject><subject>Exact sciences and technology</subject><subject>General and physical chemistry</subject><subject>Porous materials</subject><issn>0743-7463</issn><issn>1520-5827</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1999</creationdate><recordtype>article</recordtype><recordid>eNptkDtPw0AQhE8IJEKg4B-4gILCcC_fo4wCCUgRDyXUp_XZBw7GZ905EvDrcTAKDdUW8-3OziB0SvAlwZRc1aA1JkyUe2hEMorTTFG5j0ZYcpZKLtghOopxjTHWjOsRWiw7aAoIRXJfdcG_lE0yKaIPbVf5JrmGDhLnQzJ9hQC2K0P1BT-Kd8k9NL71wW9isqzqykI8RgcO6lie_M4xep7drKa36eJhfjedLFJglHcpY0r1_loDYY5unyoVoVIKxXkpMlFwbrmjVBDFIc9VTqQARYFYRRzknI3RxXDXBh9jKJ1pQ_UO4dMQbLY1mF0NPXs2sC1EC7UL0Ngq_i1orIRgPZYOWBW78mMnQ3gzQjKZmdXj0ujZfIWJouap588HHmw0a78JTR_4H_tvBnV2gA</recordid><startdate>19990803</startdate><enddate>19990803</enddate><creator>Jaroniec, Mietek</creator><creator>Kruk, Michal</creator><creator>Olivier, James P</creator><general>American Chemical Society</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>19990803</creationdate><title>Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas</title><author>Jaroniec, Mietek ; Kruk, Michal ; Olivier, James P</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a324t-338800999a13f27463e812776844e656d44c4f226184abb8b176a82a1c81fab43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1999</creationdate><topic>Chemistry</topic><topic>Colloidal state and disperse state</topic><topic>Exact sciences and technology</topic><topic>General and physical chemistry</topic><topic>Porous materials</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Jaroniec, Mietek</creatorcontrib><creatorcontrib>Kruk, Michal</creatorcontrib><creatorcontrib>Olivier, James P</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Langmuir</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Jaroniec, Mietek</au><au>Kruk, Michal</au><au>Olivier, James P</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas</atitle><jtitle>Langmuir</jtitle><addtitle>Langmuir</addtitle><date>1999-08-03</date><risdate>1999</risdate><volume>15</volume><issue>16</issue><spage>5410</spage><epage>5413</epage><pages>5410-5413</pages><issn>0743-7463</issn><eissn>1520-5827</eissn><coden>LANGD5</coden><abstract>The nitrogen adsorption isotherm measured at 77 K in the relative pressure range from about 5 × 10-7 to 0.988 for a macroporous silica is reported in a tabular form. The isotherm data are in good agreement in the high-pressure range with the reference data published by Gregg and Sing and by Kiselev and Aristov and provide an extension of the latter data to the low-pressure region, for which a reliable reference isotherm was not availalable in the literature. Application of the currently reported reference adsorption isotherm is discussed. The data can be used in comparative analysis (αs-plot or t-plot) to evaluate the external surface area, micropore volume, primary mesopore volume, and total surface area as well as to analyze surface properties of silica-based materials. The adsorption isotherm can also be applied as a statistical film thickness curve in the calculation of the mesopore size distribution.</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><doi>10.1021/la990136e</doi><tpages>4</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0743-7463 |
| ispartof | Langmuir, 1999-08, Vol.15 (16), p.5410-5413 |
| issn | 0743-7463 1520-5827 |
| language | eng |
| recordid | cdi_crossref_primary_10_1021_la990136e |
| source | American Chemical Society Journals |
| subjects | Chemistry Colloidal state and disperse state Exact sciences and technology General and physical chemistry Porous materials |
| title | Standard Nitrogen Adsorption Data for Characterization of Nanoporous Silicas |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-07T16%3A34%3A24IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-acs_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Standard%20Nitrogen%20Adsorption%20Data%20for%20Characterization%20of%20Nanoporous%20Silicas&rft.jtitle=Langmuir&rft.au=Jaroniec,%20Mietek&rft.date=1999-08-03&rft.volume=15&rft.issue=16&rft.spage=5410&rft.epage=5413&rft.pages=5410-5413&rft.issn=0743-7463&rft.eissn=1520-5827&rft.coden=LANGD5&rft_id=info:doi/10.1021/la990136e&rft_dat=%3Cacs_cross%3Ec225997204%3C/acs_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true |