Electrochemical and Scanning Force Microscopy Characterization of Fractal Palladium Surfaces Resulting from the Electroreduction of Palladium Oxide Layers

Pd oxide layers were grown by applying to smooth Pd electrodes a potential reversal technique (PRT) in 1 M H2SO4 at 25 °C. The electroreduction of the Pd oxide layer was made either voltammetrically or potentiostatically, yielding a Pd overlayer with a large increase in surface area. The effective r...

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Veröffentlicht in:Langmuir 1996-12, Vol.12 (26), p.6587-6596
Hauptverfasser: Kessler, T, Visintin, A, Bolzan, A. E, Andreasen, G, Salvarezza, R. C, Triaca, W. E, Arvia, A. J
Format: Artikel
Sprache:eng
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