Constituents of Cydonia vulgaris: Isolation and Structure Elucidation of Four New Flavonol Glycosides and Nine New α-Ionol-Derived Glycosides
In a previous paper, we described the isolation of four new sesterterpenes from Cydonia vulgaris Pers. Here we report the isolation of four new flavonol glycosides (1−4) and nine new α-ionol-derived glycosides (5−13) together with the known 3-oxo-α-ionol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranosi...
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| Veröffentlicht in: | Journal of agricultural and food chemistry 1996-07, Vol.44 (7), p.1676-1681 |
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| container_title | Journal of agricultural and food chemistry |
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| creator | De Tommasi, Nunziatina Piacente, Sonia De Simone, Francesco Pizza, Cosimo |
| description | In a previous paper, we described the isolation of four new sesterterpenes from Cydonia vulgaris Pers. Here we report the isolation of four new flavonol glycosides (1−4) and nine new α-ionol-derived glycosides (5−13) together with the known 3-oxo-α-ionol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (14), vomifoliol 9-O-β-d-glucopyranoside (roseoside) (15), and vomifoliol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (16) from the MeOH extract of the aerial parts of C. vulgaris Pers. (Rosaceae). All structures were elucidated by spectroscopic methods, including the concerted application of one-dimensional NMR and two-dimensional NMR techniques (COSY-90 and HETCOR). Keywords: Cydonia vulgaris; Rosaceae; flavonol glycosides; α-ionol glycosides; 1H and 13C NMR (one- and two-dimensional) |
| doi_str_mv | 10.1021/jf950547a |
| format | Article |
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Here we report the isolation of four new flavonol glycosides (1−4) and nine new α-ionol-derived glycosides (5−13) together with the known 3-oxo-α-ionol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (14), vomifoliol 9-O-β-d-glucopyranoside (roseoside) (15), and vomifoliol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (16) from the MeOH extract of the aerial parts of C. vulgaris Pers. (Rosaceae). All structures were elucidated by spectroscopic methods, including the concerted application of one-dimensional NMR and two-dimensional NMR techniques (COSY-90 and HETCOR). 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Agric. Food Chem</addtitle><description>In a previous paper, we described the isolation of four new sesterterpenes from Cydonia vulgaris Pers. Here we report the isolation of four new flavonol glycosides (1−4) and nine new α-ionol-derived glycosides (5−13) together with the known 3-oxo-α-ionol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (14), vomifoliol 9-O-β-d-glucopyranoside (roseoside) (15), and vomifoliol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (16) from the MeOH extract of the aerial parts of C. vulgaris Pers. (Rosaceae). All structures were elucidated by spectroscopic methods, including the concerted application of one-dimensional NMR and two-dimensional NMR techniques (COSY-90 and HETCOR). 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Psychology</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>De Tommasi, Nunziatina</creatorcontrib><creatorcontrib>Piacente, Sonia</creatorcontrib><creatorcontrib>De Simone, Francesco</creatorcontrib><creatorcontrib>Pizza, Cosimo</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Journal of agricultural and food chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>De Tommasi, Nunziatina</au><au>Piacente, Sonia</au><au>De Simone, Francesco</au><au>Pizza, Cosimo</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Constituents of Cydonia vulgaris: Isolation and Structure Elucidation of Four New Flavonol Glycosides and Nine New α-Ionol-Derived Glycosides</atitle><jtitle>Journal of agricultural and food chemistry</jtitle><addtitle>J. Agric. Food Chem</addtitle><date>1996-07-18</date><risdate>1996</risdate><volume>44</volume><issue>7</issue><spage>1676</spage><epage>1681</epage><pages>1676-1681</pages><issn>0021-8561</issn><eissn>1520-5118</eissn><coden>JAFCAU</coden><abstract>In a previous paper, we described the isolation of four new sesterterpenes from Cydonia vulgaris Pers. Here we report the isolation of four new flavonol glycosides (1−4) and nine new α-ionol-derived glycosides (5−13) together with the known 3-oxo-α-ionol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (14), vomifoliol 9-O-β-d-glucopyranoside (roseoside) (15), and vomifoliol 9-O-β-d-apiofuranosyl-(1→6)-β-d-glucopyranoside (16) from the MeOH extract of the aerial parts of C. vulgaris Pers. (Rosaceae). All structures were elucidated by spectroscopic methods, including the concerted application of one-dimensional NMR and two-dimensional NMR techniques (COSY-90 and HETCOR). Keywords: Cydonia vulgaris; Rosaceae; flavonol glycosides; α-ionol glycosides; 1H and 13C NMR (one- and two-dimensional)</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><doi>10.1021/jf950547a</doi><tpages>6</tpages></addata></record> |
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| identifier | ISSN: 0021-8561 |
| ispartof | Journal of agricultural and food chemistry, 1996-07, Vol.44 (7), p.1676-1681 |
| issn | 0021-8561 1520-5118 |
| language | eng |
| recordid | cdi_crossref_primary_10_1021_jf950547a |
| source | American Chemical Society Journals |
| subjects | Aroma and flavouring agent industries Biological and medical sciences Food industries Fundamental and applied biological sciences. Psychology |
| title | Constituents of Cydonia vulgaris: Isolation and Structure Elucidation of Four New Flavonol Glycosides and Nine New α-Ionol-Derived Glycosides |
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