Characterization of Nitrogen-Containing Species in Coal- and Petroleum-Derived Products by Ammonia Chemical Ionization High-Resolution Mass Spectrometry
A coal-derived light distillate and a petroleum-derived residuum have been studied by high-resolution mass spectrometry using both low-pressure ammonia chemical ionization and low-voltage electron impact ionization. A mass calibration mixture for use with ammonia chemical ionization has been develop...
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| Veröffentlicht in: | Energy & fuels 1997-01, Vol.11 (1), p.137-143 |
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| container_title | Energy & fuels |
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| creator | Veloski, Garret A Lynn, Ronald J Sprecher, Richard F |
| description | A coal-derived light distillate and a petroleum-derived residuum have been studied by high-resolution mass spectrometry using both low-pressure ammonia chemical ionization and low-voltage electron impact ionization. A mass calibration mixture for use with ammonia chemical ionization has been developed. Selective ionization of the basic nitrogen-containing compounds by ammonia chemical ionization and compound type characterization of the resulting quasi-molecular species has been demonstrated. Several homologous series of N-containing compounds were identified in a basic extract by electron impact ionization and compared with quasi-molecular analogs identified by ammonia chemical ionization. |
| doi_str_mv | 10.1021/ef9601069 |
| format | Article |
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A mass calibration mixture for use with ammonia chemical ionization has been developed. Selective ionization of the basic nitrogen-containing compounds by ammonia chemical ionization and compound type characterization of the resulting quasi-molecular species has been demonstrated. Several homologous series of N-containing compounds were identified in a basic extract by electron impact ionization and compared with quasi-molecular analogs identified by ammonia chemical ionization.</description><identifier>ISSN: 0887-0624</identifier><identifier>EISSN: 1520-5029</identifier><identifier>DOI: 10.1021/ef9601069</identifier><identifier>CODEN: ENFUEM</identifier><language>eng</language><publisher>Washington, DC: American Chemical Society</publisher><subject>Applied sciences ; Energy ; Exact sciences and technology ; Fuel processing. 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A mass calibration mixture for use with ammonia chemical ionization has been developed. Selective ionization of the basic nitrogen-containing compounds by ammonia chemical ionization and compound type characterization of the resulting quasi-molecular species has been demonstrated. Several homologous series of N-containing compounds were identified in a basic extract by electron impact ionization and compared with quasi-molecular analogs identified by ammonia chemical ionization.</description><subject>Applied sciences</subject><subject>Energy</subject><subject>Exact sciences and technology</subject><subject>Fuel processing. Carbochemistry and petrochemistry</subject><subject>Fuels</subject><subject>Liquid petroleum product processing</subject><subject>Solid fuel processing (coal, coke, brown coal, peat, wood, etc.)</subject><issn>0887-0624</issn><issn>1520-5029</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1997</creationdate><recordtype>article</recordtype><recordid>eNptkM9O3DAQxq2qSN0CB97Ah_bQg8F2Yic-0rRlkYBS_vRqTRxn1zSxV3a2YnmSPi6GRXvqafTN_Ob7NIPQEaPHjHJ2YnslKaNSvUMzJjglgnL1Hs1oXVeESl5-QB9TeqCUyqIWM_SvWUIEM9nonmBywePQ4ys3xbCwnjTBT-C88wt8u7LG2YSdx02AgWDwHb62GRzseiTfssFfmzsxdGszJdxu8Ok4Bu8AN0s7OgMDPs_yLWXuFktyY1MY1q_6ElJ6zciGY3bdHKC9HoZkD9_qPrr_8f2umZOLn2fnzekFgUKoiQhegzVGdl0prGDAOC07wZgF1Va8Knir2rarZAuUgWxZV0vZyqq3ValkrYpiH33Z-poYUoq216voRogbzah-eanevTSzn7bsClK-p4_gjUu7BS5KUQuWMbLFXJrs424M8Y-WVVEJfXd9q78ycTn_VSj9O_OftzyYpB_COvp88H_inwHvtpNy</recordid><startdate>19970101</startdate><enddate>19970101</enddate><creator>Veloski, Garret A</creator><creator>Lynn, Ronald J</creator><creator>Sprecher, Richard F</creator><general>American Chemical Society</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>19970101</creationdate><title>Characterization of Nitrogen-Containing Species in Coal- and Petroleum-Derived Products by Ammonia Chemical Ionization High-Resolution Mass Spectrometry</title><author>Veloski, Garret A ; Lynn, Ronald J ; Sprecher, Richard F</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a359t-528aecc6dd45e51a1204d511ea9b72732b9bbd76ba01a6b1d866b67fe74968933</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1997</creationdate><topic>Applied sciences</topic><topic>Energy</topic><topic>Exact sciences and technology</topic><topic>Fuel processing. Carbochemistry and petrochemistry</topic><topic>Fuels</topic><topic>Liquid petroleum product processing</topic><topic>Solid fuel processing (coal, coke, brown coal, peat, wood, etc.)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Veloski, Garret A</creatorcontrib><creatorcontrib>Lynn, Ronald J</creatorcontrib><creatorcontrib>Sprecher, Richard F</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Energy & fuels</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Veloski, Garret A</au><au>Lynn, Ronald J</au><au>Sprecher, Richard F</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Characterization of Nitrogen-Containing Species in Coal- and Petroleum-Derived Products by Ammonia Chemical Ionization High-Resolution Mass Spectrometry</atitle><jtitle>Energy & fuels</jtitle><addtitle>Energy Fuels</addtitle><date>1997-01-01</date><risdate>1997</risdate><volume>11</volume><issue>1</issue><spage>137</spage><epage>143</epage><pages>137-143</pages><issn>0887-0624</issn><eissn>1520-5029</eissn><coden>ENFUEM</coden><abstract>A coal-derived light distillate and a petroleum-derived residuum have been studied by high-resolution mass spectrometry using both low-pressure ammonia chemical ionization and low-voltage electron impact ionization. A mass calibration mixture for use with ammonia chemical ionization has been developed. Selective ionization of the basic nitrogen-containing compounds by ammonia chemical ionization and compound type characterization of the resulting quasi-molecular species has been demonstrated. Several homologous series of N-containing compounds were identified in a basic extract by electron impact ionization and compared with quasi-molecular analogs identified by ammonia chemical ionization.</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><doi>10.1021/ef9601069</doi><tpages>7</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0887-0624 |
| ispartof | Energy & fuels, 1997-01, Vol.11 (1), p.137-143 |
| issn | 0887-0624 1520-5029 |
| language | eng |
| recordid | cdi_crossref_primary_10_1021_ef9601069 |
| source | American Chemical Society Publications |
| subjects | Applied sciences Energy Exact sciences and technology Fuel processing. Carbochemistry and petrochemistry Fuels Liquid petroleum product processing Solid fuel processing (coal, coke, brown coal, peat, wood, etc.) |
| title | Characterization of Nitrogen-Containing Species in Coal- and Petroleum-Derived Products by Ammonia Chemical Ionization High-Resolution Mass Spectrometry |
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