Mixed Silica Titania Materials Prepared from a Single-Source Sol−Gel Precursor: A Time-Resolved SAXS Study of the Gelation, Aging, Supercritical Drying, and Calcination Processes
The morphology of gels prepared from a silica/titania single-source precursor (1), obtained by reaction of 3-oxoethyl-6-trimethoxysilyl-hexan-2-one with Ti(OiPr)4, was investigated by small-angle X-ray scattering (SAXS) through all stages of the preparation process, that is, gelation, aging, drying,...
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Veröffentlicht in: | Chemistry of materials 2005-06, Vol.17 (12), p.3146-3153 |
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Hauptverfasser: | , , , , , , , , |
Format: | Artikel |
Sprache: | eng |
Online-Zugang: | Volltext |
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