Synthesis of 1 nm Pd Nanoparticles in a Microfluidic Reactor: Insights from in Situ X‑ray Absorption Fine Structure Spectroscopy and Small-Angle X‑ray Scattering

A novel microfluidic reactor for in situ small-angle X-ray scattering (SAXS) and X-ray absorption fine structure spectroscopy (XAFS) of Pd colloidal nanoparticles synthesis is reported. The microreactor allows time resolution ranging from milliseconds to several minutes with a residence time of over...

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Veröffentlicht in:Journal of Physical Chemistry C, 119(23):13257–13267 119(23):13257–13267, 2015-06, Vol.119 (23), p.13264-13274
Hauptverfasser: Karim, Ayman M, Al Hasan, Naila, Ivanov, Sergei, Siefert, Soenke, Kelly, Ryan T, Hallfors, Nicholas G, Benavidez, Angelica, Kovarik, Libor, Jenkins, Aaron, Winans, Randall E, Datye, Abhaya K
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Sprache:eng
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