Tree Ring Wood Analysis after Hydrogen Peroxide Pressure Decomposition with Inductively Coupled Plasma Atomic Emission Spectrometry and Electrothermal Vaporization
A method utilizing pressure decomposition to minimize sample pretreatment is described for the inductively coupled plasma atomic emission spectrometric analysis of red spruce and sugar maple. Cores collected from trees growing on Camels Hump Mountain, Vermont, were divided into decade increments in...
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| Veröffentlicht in: | Anal. Chem.; (United States) 1985-02, Vol.57 (2), p.406-411 |
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| creator | Matusiewicz, Henryk Barnes, Ramon M |
| description | A method utilizing pressure decomposition to minimize sample pretreatment is described for the inductively coupled plasma atomic emission spectrometric analysis of red spruce and sugar maple. Cores collected from trees growing on Camels Hump Mountain, Vermont, were divided into decade increments in order to monitor the temporal changes in concentrations of 21 elements. Dried wood samples were decomposed in a bomb made of Teflon with 50% hydrogen peroxide heated in an oven at 125/sup 0/C for 4 h. The digestion permitted use of aqueous standards and minimized any potential matrix effects. The element concentrations were obtained sequentially by electrothermal vaporization ICP-AES using 5 ..mu..L sample aliquots. The method precision varied between 3 and 12%. Elements forming oxyanions (Al, As, Fe, Ge, Mn, Si, V) were found at elevated concentrations during the most recent three decades, while other metal (e.g., Mg, Zn) concentrations were unchanged or decreased. 45 references, 6 tables, 1 figure. |
| doi_str_mv | 10.1021/ac50001a019 |
| format | Article |
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Cores collected from trees growing on Camels Hump Mountain, Vermont, were divided into decade increments in order to monitor the temporal changes in concentrations of 21 elements. Dried wood samples were decomposed in a bomb made of Teflon with 50% hydrogen peroxide heated in an oven at 125/sup 0/C for 4 h. The digestion permitted use of aqueous standards and minimized any potential matrix effects. The element concentrations were obtained sequentially by electrothermal vaporization ICP-AES using 5 ..mu..L sample aliquots. The method precision varied between 3 and 12%. Elements forming oxyanions (Al, As, Fe, Ge, Mn, Si, V) were found at elevated concentrations during the most recent three decades, while other metal (e.g., Mg, Zn) concentrations were unchanged or decreased. 45 references, 6 tables, 1 figure.</description><identifier>ISSN: 0003-2700</identifier><identifier>EISSN: 1520-6882</identifier><identifier>DOI: 10.1021/ac50001a019</identifier><identifier>CODEN: ANCHAM</identifier><language>eng</language><publisher>Washington, DC: American Chemical Society</publisher><subject>400104 - Spectral Procedures- (-1987) ; 500200 - Environment, Atmospheric- Chemicals Monitoring & Transport- (-1989) ; AIR POLLUTION ; AIR POLLUTION MONITORS ; ALKALI METALS ; ALKALINE EARTH METALS ; ALUMINIUM ; Analytical chemistry ; ARSENIC ; BARIUM ; BERYLLIUM ; BORON ; CADMIUM ; CALCIUM ; CHEMICAL ANALYSIS ; Chemistry ; COPPER ; DATA ; ELECTRIC FURNACES ; ELEMENTS ; EMISSION SPECTROSCOPY ; ENVIRONMENTAL SCIENCES ; Exact sciences and technology ; EXPERIMENTAL DATA ; FURNACES ; GERMANIUM ; HYDROGEN COMPOUNDS ; HYDROGEN PEROXIDE ; INFORMATION ; INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY ; ION SOURCES ; IRON ; LEAD ; LITHIUM ; MAGNESIUM ; MANGANESE ; MEASURING INSTRUMENTS ; MEDIUM TEMPERATURE ; METALS ; MONITORS ; NUMERICAL DATA ; OXYGEN COMPOUNDS ; PEROXIDES ; PLASMA ; POLLUTION ; POTASSIUM ; QUANTITATIVE CHEMICAL ANALYSIS ; SELENIUM ; SEMIMETALS ; SILICON ; SODIUM ; Spectrometric and optical methods ; SPECTROSCOPY ; STRONTIUM ; TRACE AMOUNTS ; TRANSITION ELEMENTS ; VANADIUM ; WOOD ; ZINC</subject><ispartof>Anal. Chem.; (United States), 1985-02, Vol.57 (2), p.406-411</ispartof><rights>1985 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a357t-8f98eacf8aee76510a7b5cda02b1d78bae31cab267cba4daba589da6ffe740b33</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://pubs.acs.org/doi/pdf/10.1021/ac50001a019$$EPDF$$P50$$Gacs$$H</linktopdf><linktohtml>$$Uhttps://pubs.acs.org/doi/10.1021/ac50001a019$$EHTML$$P50$$Gacs$$H</linktohtml><link.rule.ids>314,780,784,885,2765,27076,27924,27925,56738,56788</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=9046311$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/biblio/5929053$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Matusiewicz, Henryk</creatorcontrib><creatorcontrib>Barnes, Ramon M</creatorcontrib><creatorcontrib>Univ. of Massachusetts, Amherst</creatorcontrib><title>Tree Ring Wood Analysis after Hydrogen Peroxide Pressure Decomposition with Inductively Coupled Plasma Atomic Emission Spectrometry and Electrothermal Vaporization</title><title>Anal. Chem.; (United States)</title><addtitle>Anal. Chem</addtitle><description>A method utilizing pressure decomposition to minimize sample pretreatment is described for the inductively coupled plasma atomic emission spectrometric analysis of red spruce and sugar maple. Cores collected from trees growing on Camels Hump Mountain, Vermont, were divided into decade increments in order to monitor the temporal changes in concentrations of 21 elements. Dried wood samples were decomposed in a bomb made of Teflon with 50% hydrogen peroxide heated in an oven at 125/sup 0/C for 4 h. The digestion permitted use of aqueous standards and minimized any potential matrix effects. The element concentrations were obtained sequentially by electrothermal vaporization ICP-AES using 5 ..mu..L sample aliquots. The method precision varied between 3 and 12%. Elements forming oxyanions (Al, As, Fe, Ge, Mn, Si, V) were found at elevated concentrations during the most recent three decades, while other metal (e.g., Mg, Zn) concentrations were unchanged or decreased. 45 references, 6 tables, 1 figure.</description><subject>400104 - Spectral Procedures- (-1987)</subject><subject>500200 - Environment, Atmospheric- Chemicals Monitoring & Transport- (-1989)</subject><subject>AIR POLLUTION</subject><subject>AIR POLLUTION MONITORS</subject><subject>ALKALI METALS</subject><subject>ALKALINE EARTH METALS</subject><subject>ALUMINIUM</subject><subject>Analytical chemistry</subject><subject>ARSENIC</subject><subject>BARIUM</subject><subject>BERYLLIUM</subject><subject>BORON</subject><subject>CADMIUM</subject><subject>CALCIUM</subject><subject>CHEMICAL ANALYSIS</subject><subject>Chemistry</subject><subject>COPPER</subject><subject>DATA</subject><subject>ELECTRIC FURNACES</subject><subject>ELEMENTS</subject><subject>EMISSION SPECTROSCOPY</subject><subject>ENVIRONMENTAL SCIENCES</subject><subject>Exact sciences and technology</subject><subject>EXPERIMENTAL DATA</subject><subject>FURNACES</subject><subject>GERMANIUM</subject><subject>HYDROGEN COMPOUNDS</subject><subject>HYDROGEN PEROXIDE</subject><subject>INFORMATION</subject><subject>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</subject><subject>ION SOURCES</subject><subject>IRON</subject><subject>LEAD</subject><subject>LITHIUM</subject><subject>MAGNESIUM</subject><subject>MANGANESE</subject><subject>MEASURING INSTRUMENTS</subject><subject>MEDIUM TEMPERATURE</subject><subject>METALS</subject><subject>MONITORS</subject><subject>NUMERICAL DATA</subject><subject>OXYGEN COMPOUNDS</subject><subject>PEROXIDES</subject><subject>PLASMA</subject><subject>POLLUTION</subject><subject>POTASSIUM</subject><subject>QUANTITATIVE CHEMICAL ANALYSIS</subject><subject>SELENIUM</subject><subject>SEMIMETALS</subject><subject>SILICON</subject><subject>SODIUM</subject><subject>Spectrometric and optical methods</subject><subject>SPECTROSCOPY</subject><subject>STRONTIUM</subject><subject>TRACE AMOUNTS</subject><subject>TRANSITION ELEMENTS</subject><subject>VANADIUM</subject><subject>WOOD</subject><subject>ZINC</subject><issn>0003-2700</issn><issn>1520-6882</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1985</creationdate><recordtype>article</recordtype><recordid>eNpt0c1u1DAQB_AIgcRSOPECFkLigFLsZJ2P47IstNKqRO1SjtbEnnRdkjjyeKHhdXjRZgmqeuA00sxvRiP9o-i14KeCJ-IDaMk5F8BF-SRaCJnwOCuK5Gm0mNppnOScP49eEN1OSHCRLaI_O4_ILm1_w747Z9iqh3YkSwyagJ6djca7G-xZhd7dWYOs8kh08Mg-oXbd4MgG63r2y4Y9O-_NQQf7E9uRrd1haNGwqgXqgK2C66xmm84SHf3VgDp412HwI4PesE37txH26Dto2TUMztvfcDz-MnrWQEv46l89ib593uzWZ_H265fz9WobQyrzEBdNWSDopgDEPJOCQ15LbYAntTB5UQOmQkOdZLmuYWmgBlmUBrKmwXzJ6zQ9id7Mdx0Fq0jbgHqvXd9PnylZJiWXR_R-Rto7Io-NGrztwI9KcHUMQT0KYdJvZz0AaWgbD7229LBS8mWWCjGxeGaWAt49jMH_UFme5lLtqiv1UW6vs4pfqMvJv5s9aFK37uCn1Oi_D9wDtIinfA</recordid><startdate>19850201</startdate><enddate>19850201</enddate><creator>Matusiewicz, Henryk</creator><creator>Barnes, Ramon M</creator><general>American Chemical Society</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>OTOTI</scope></search><sort><creationdate>19850201</creationdate><title>Tree Ring Wood Analysis after Hydrogen Peroxide Pressure Decomposition with Inductively Coupled Plasma Atomic Emission Spectrometry and Electrothermal Vaporization</title><author>Matusiewicz, Henryk ; Barnes, Ramon M</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a357t-8f98eacf8aee76510a7b5cda02b1d78bae31cab267cba4daba589da6ffe740b33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1985</creationdate><topic>400104 - Spectral Procedures- (-1987)</topic><topic>500200 - Environment, Atmospheric- Chemicals Monitoring & Transport- (-1989)</topic><topic>AIR POLLUTION</topic><topic>AIR POLLUTION MONITORS</topic><topic>ALKALI METALS</topic><topic>ALKALINE EARTH METALS</topic><topic>ALUMINIUM</topic><topic>Analytical chemistry</topic><topic>ARSENIC</topic><topic>BARIUM</topic><topic>BERYLLIUM</topic><topic>BORON</topic><topic>CADMIUM</topic><topic>CALCIUM</topic><topic>CHEMICAL ANALYSIS</topic><topic>Chemistry</topic><topic>COPPER</topic><topic>DATA</topic><topic>ELECTRIC FURNACES</topic><topic>ELEMENTS</topic><topic>EMISSION SPECTROSCOPY</topic><topic>ENVIRONMENTAL SCIENCES</topic><topic>Exact sciences and technology</topic><topic>EXPERIMENTAL DATA</topic><topic>FURNACES</topic><topic>GERMANIUM</topic><topic>HYDROGEN COMPOUNDS</topic><topic>HYDROGEN PEROXIDE</topic><topic>INFORMATION</topic><topic>INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY</topic><topic>ION SOURCES</topic><topic>IRON</topic><topic>LEAD</topic><topic>LITHIUM</topic><topic>MAGNESIUM</topic><topic>MANGANESE</topic><topic>MEASURING INSTRUMENTS</topic><topic>MEDIUM TEMPERATURE</topic><topic>METALS</topic><topic>MONITORS</topic><topic>NUMERICAL DATA</topic><topic>OXYGEN COMPOUNDS</topic><topic>PEROXIDES</topic><topic>PLASMA</topic><topic>POLLUTION</topic><topic>POTASSIUM</topic><topic>QUANTITATIVE CHEMICAL ANALYSIS</topic><topic>SELENIUM</topic><topic>SEMIMETALS</topic><topic>SILICON</topic><topic>SODIUM</topic><topic>Spectrometric and optical methods</topic><topic>SPECTROSCOPY</topic><topic>STRONTIUM</topic><topic>TRACE AMOUNTS</topic><topic>TRANSITION ELEMENTS</topic><topic>VANADIUM</topic><topic>WOOD</topic><topic>ZINC</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Matusiewicz, Henryk</creatorcontrib><creatorcontrib>Barnes, Ramon M</creatorcontrib><creatorcontrib>Univ. of Massachusetts, Amherst</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>OSTI.GOV</collection><jtitle>Anal. Chem.; (United States)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Matusiewicz, Henryk</au><au>Barnes, Ramon M</au><aucorp>Univ. of Massachusetts, Amherst</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Tree Ring Wood Analysis after Hydrogen Peroxide Pressure Decomposition with Inductively Coupled Plasma Atomic Emission Spectrometry and Electrothermal Vaporization</atitle><jtitle>Anal. Chem.; (United States)</jtitle><addtitle>Anal. Chem</addtitle><date>1985-02-01</date><risdate>1985</risdate><volume>57</volume><issue>2</issue><spage>406</spage><epage>411</epage><pages>406-411</pages><issn>0003-2700</issn><eissn>1520-6882</eissn><coden>ANCHAM</coden><abstract>A method utilizing pressure decomposition to minimize sample pretreatment is described for the inductively coupled plasma atomic emission spectrometric analysis of red spruce and sugar maple. Cores collected from trees growing on Camels Hump Mountain, Vermont, were divided into decade increments in order to monitor the temporal changes in concentrations of 21 elements. Dried wood samples were decomposed in a bomb made of Teflon with 50% hydrogen peroxide heated in an oven at 125/sup 0/C for 4 h. The digestion permitted use of aqueous standards and minimized any potential matrix effects. The element concentrations were obtained sequentially by electrothermal vaporization ICP-AES using 5 ..mu..L sample aliquots. The method precision varied between 3 and 12%. Elements forming oxyanions (Al, As, Fe, Ge, Mn, Si, V) were found at elevated concentrations during the most recent three decades, while other metal (e.g., Mg, Zn) concentrations were unchanged or decreased. 45 references, 6 tables, 1 figure.</abstract><cop>Washington, DC</cop><pub>American Chemical Society</pub><doi>10.1021/ac50001a019</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
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| ispartof | Anal. Chem.; (United States), 1985-02, Vol.57 (2), p.406-411 |
| issn | 0003-2700 1520-6882 |
| language | eng |
| recordid | cdi_crossref_primary_10_1021_ac50001a019 |
| source | ACS_美国化学学会期刊（与NSTL共建） |
| subjects | 400104 - Spectral Procedures- (-1987) 500200 - Environment, Atmospheric- Chemicals Monitoring & Transport- (-1989) AIR POLLUTION AIR POLLUTION MONITORS ALKALI METALS ALKALINE EARTH METALS ALUMINIUM Analytical chemistry ARSENIC BARIUM BERYLLIUM BORON CADMIUM CALCIUM CHEMICAL ANALYSIS Chemistry COPPER DATA ELECTRIC FURNACES ELEMENTS EMISSION SPECTROSCOPY ENVIRONMENTAL SCIENCES Exact sciences and technology EXPERIMENTAL DATA FURNACES GERMANIUM HYDROGEN COMPOUNDS HYDROGEN PEROXIDE INFORMATION INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY ION SOURCES IRON LEAD LITHIUM MAGNESIUM MANGANESE MEASURING INSTRUMENTS MEDIUM TEMPERATURE METALS MONITORS NUMERICAL DATA OXYGEN COMPOUNDS PEROXIDES PLASMA POLLUTION POTASSIUM QUANTITATIVE CHEMICAL ANALYSIS SELENIUM SEMIMETALS SILICON SODIUM Spectrometric and optical methods SPECTROSCOPY STRONTIUM TRACE AMOUNTS TRANSITION ELEMENTS VANADIUM WOOD ZINC |
| title | Tree Ring Wood Analysis after Hydrogen Peroxide Pressure Decomposition with Inductively Coupled Plasma Atomic Emission Spectrometry and Electrothermal Vaporization |
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