High-Resolution Capillary Tube NMR. A Miniaturized 5-μL High-Sensitivity TXI Probe for Mass-Limited Samples, Off-Line LC NMR, and HT NMR

A new triple-resonance (TXI) (1H, 13C, 15N) high-resolution nuclear magnetic resonance (NMR) capillary probe with 2.5-μL NMR-active sample volume (V obs) was built and tested for applications with mass- and volume-limited samples and for coupling of microbore liquid chromatography to NMR. This is th...

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Veröffentlicht in:	Analytical chemistry (Washington) 2002-09, Vol.74 (17), p.4464-4471
Hauptverfasser:	Schlotterbeck, Götz, Ross, Alfred, Hochstrasser, Remo, Senn, Hans, Kühn, Till, Marek, Daniel, Schett, Oscar
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Chemistry Exact sciences and technology Spectrometric and optical methods
Online-Zugang:	Volltext
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