Determination of carbonyl sulfide in air by derivatization with 1,3-diaminopropane and capillary gas chromatographic analysis

A method for monitoring personal exposure to carbonyl sulfide in air has been developed and validated. Carbonyl sulfide is collected on Woelm column chromatography polyamide coated with 1,3-diaminopropane as an in situ derivatizing agent. This is followed by desorption with 0.01 N NaOH solution and...

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Veröffentlicht in:	Anal. Chem.; (United States) 1985-12, Vol.57 (14), p.2792-2796
Hauptverfasser:	Leiber, Mark A, Berk, Howard C
Format:	Artikel
Sprache:	eng
Schlagworte:	400102 - Chemical & Spectral Procedures 500200 - Environment, Atmospheric- Chemicals Monitoring & Transport- (-1989) AIR AIR POLLUTION MONITORING AIR POLLUTION MONITORS Analytical chemistry CAPILLARY FLOW CARBONYLS CHALCOGENIDES CHEMICAL ANALYSIS CHEMICAL REACTIONS Chemistry Chromatographic methods and physical methods associated with chromatography CHROMATOGRAPHY DATA DERIVATIZATION DESORPTION ENVIRONMENTAL SCIENCES Exact sciences and technology EXPERIMENTAL DATA FLUID FLOW FLUIDS Gas chromatographic methods GAS CHROMATOGRAPHY GASES HUMIDITY INFORMATION INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY MEASURING INSTRUMENTS MONITORS NUMERICAL DATA QUANTITATIVE CHEMICAL ANALYSIS SEPARATION PROCESSES STORAGE SULFIDES SULFUR COMPOUNDS TEMPERATURE DEPENDENCE
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