Determination of phenols in a coal liquefaction product by gas chromatography and combined gas chromatography-mass spectrometry

The phenolic fraction of a SRC-II middle distillate was isolated and the individual phenolic constituents further separated and identified by using gas chromatography and combined gas chromatography/mass spectrometry. This complex mixture of phenols was separated with a high-resolution fused-silica...

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Veröffentlicht in:	Anal. Chem.; (United States) 1982-08, Vol.54 (9), p.1570-1572
Hauptverfasser:	White, Curt M, Li, Norman C
Format:	Artikel
Sprache:	eng
Schlagworte:	01 COAL, LIGNITE, AND PEAT 010600 - Coal, Lignite, & Peat- Properties & Composition 400105 - Separation Procedures AROMATICS CHEMICAL ANALYSIS CHROMATOGRAPHY COAL LIQUEFACTION COAL LIQUIDS DISTILLATES FLUIDS GAS CHROMATOGRAPHY HYDROXY COMPOUNDS INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY LIQUEFACTION LIQUIDS MASS SPECTRA MASS SPECTROSCOPY ORGANIC COMPOUNDS PHENOLS QUALITATIVE CHEMICAL ANALYSIS SEPARATION PROCESSES SPECTRA SPECTROSCOPY SRC-II PROCESS THERMOCHEMICAL PROCESSES
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container_title	Anal. Chem.; (United States)
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creator	White, Curt M Li, Norman C
description	The phenolic fraction of a SRC-II middle distillate was isolated and the individual phenolic constituents further separated and identified by using gas chromatography and combined gas chromatography/mass spectrometry. This complex mixture of phenols was separated with a high-resolution fused-silica capillary column wall-coated with Superox-20M. Identification of 29 compounds was possible. All compounds except one were identified by using two identification parameters: (1) cochromatography with authentic standards and (2) matching mass spectra. All major and most minor constituents have been identified.
doi_str_mv	10.1021/ac00246a025
format	Article
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This complex mixture of phenols was separated with a high-resolution fused-silica capillary column wall-coated with Superox-20M. Identification of 29 compounds was possible. All compounds except one were identified by using two identification parameters: (1) cochromatography with authentic standards and (2) matching mass spectra. All major and most minor constituents have been identified.</abstract><cop>United States</cop><pub>American Chemical Society</pub><doi>10.1021/ac00246a025</doi><tpages>3</tpages></addata></record>
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subjects	01 COAL, LIGNITE, AND PEAT 010600 - Coal, Lignite, & Peat- Properties & Composition 400105 - Separation Procedures AROMATICS CHEMICAL ANALYSIS CHROMATOGRAPHY COAL LIQUEFACTION COAL LIQUIDS DISTILLATES FLUIDS GAS CHROMATOGRAPHY HYDROXY COMPOUNDS INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY LIQUEFACTION LIQUIDS MASS SPECTRA MASS SPECTROSCOPY ORGANIC COMPOUNDS PHENOLS QUALITATIVE CHEMICAL ANALYSIS SEPARATION PROCESSES SPECTRA SPECTROSCOPY SRC-II PROCESS THERMOCHEMICAL PROCESSES
title	Determination of phenols in a coal liquefaction product by gas chromatography and combined gas chromatography-mass spectrometry
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