Hydrothermal Synthesis, Structure, and Characterization of a Mixed-Valent Iron(II/III) Phosphate, NaFe3.67(PO4)3: A New Variation of the Alluaudite Structure Type

A mixed-valent Fe(II/III) phosphate, NaFe3.67(PO4)3, has been synthesized by high-temperature/high-pressure hydrothermal methods and characterized by single-crystal X-ray diffraction, EDAX, magnetic susceptibility, Mössbauer, infrared, and diffuse reflectance spectroscopies, DTA, and bond valence su...

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Veröffentlicht in:	Journal of solid state chemistry 1998-08, Vol.139 (1), p.152-160
Hauptverfasser:	Korzenski, Michael B., Schimek, George L., Kolis, Joseph W., Long, Gary J.
Format:	Artikel
Sprache:	eng
Schlagworte:	Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Inorganic compounds Magnetic properties and materials Magnetic resonances and relaxations in condensed matter, mössbauer effect Magnetically ordered materials: other intrinsic properties Mossbauer effect other γ-ray spectroscopy Mössbauer effect other γ-ray spectroscopy Physics Salts Saturation moments and magnetic susceptibilities Structure of solids and liquids crystallography Structure of specific crystalline solids
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