High‐induction nanocrystalline soft magnetic Fe X Ti Y B Z films prepared by magnetron sputtering
To design films with the Fe/TiB 2 nanocomposite structure, which are characterized by high saturation induction B s , the phase and structural states and static magnetic properties of Fe‐TiB 2 films prepared by magnetron sputtering and subjected to subsequent annealing have been studied. According t...
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| Veröffentlicht in: | Physica status solidi. C 2016-12, Vol.13 (10-12), p.965-971 |
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| creator | Sheftel, Elena N. Tedzhetov, Valentin A. Harin, Eugene V. Kiryukhantsev‐Korneev, Filipp V. Usmanova, Galina Sh |
| description | To design films with the Fe/TiB
2
nanocomposite structure, which are characterized by high saturation induction
B
s
, the phase and structural states and static magnetic properties of Fe‐TiB
2
films prepared by magnetron sputtering and subjected to subsequent annealing have been studied. According to X‐ray diffraction data, either amorphous or nanocrystalline single‐phase structure (an α‐Fe(Ti,B) supersaturated solid solution with a bcc crystal lattice) is formed in the as‐sputtered films. Depending on the film composition, the grain size of the α‐Fe(Ti,B) phase varies from 45.6 to 6.5 nm; grains are characterized by high microstrain (0.21‐4.96%). The annealing at 200‐500 °C leads to a decrease in the lattice parameter of the α‐Fe(Ti,B) phase, i.e. to its depletion of titanium and boron and to the formation of two‐phase α‐Fe + Fe
3
B structure after annealing at 500 °C. The annealing at 200‐500 °C almost does not affect the grain size and microstrain of the bcc α‐Fe‐based phase. The amorphous state of the films is stable up to 500 °C. All studied films are ferromagnets; the saturation induction
B
s
(0.95‐2.13 T) and coercive field
H
c
(0.4‐5 kA/m) of the films were determined. Correlations between the
B
s
and
H
c
magnitudes and the chemical composition of the films, their phase and structural states and magnetic structure are discussed. (© 2016 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim) |
| doi_str_mv | 10.1002/pssc.201600107 |
| format | Article |
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2
nanocomposite structure, which are characterized by high saturation induction
B
s
, the phase and structural states and static magnetic properties of Fe‐TiB
2
films prepared by magnetron sputtering and subjected to subsequent annealing have been studied. According to X‐ray diffraction data, either amorphous or nanocrystalline single‐phase structure (an α‐Fe(Ti,B) supersaturated solid solution with a bcc crystal lattice) is formed in the as‐sputtered films. Depending on the film composition, the grain size of the α‐Fe(Ti,B) phase varies from 45.6 to 6.5 nm; grains are characterized by high microstrain (0.21‐4.96%). The annealing at 200‐500 °C leads to a decrease in the lattice parameter of the α‐Fe(Ti,B) phase, i.e. to its depletion of titanium and boron and to the formation of two‐phase α‐Fe + Fe
3
B structure after annealing at 500 °C. The annealing at 200‐500 °C almost does not affect the grain size and microstrain of the bcc α‐Fe‐based phase. The amorphous state of the films is stable up to 500 °C. All studied films are ferromagnets; the saturation induction
B
s
(0.95‐2.13 T) and coercive field
H
c
(0.4‐5 kA/m) of the films were determined. Correlations between the
B
s
and
H
c
magnitudes and the chemical composition of the films, their phase and structural states and magnetic structure are discussed. (© 2016 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)</description><identifier>ISSN: 1862-6351</identifier><identifier>EISSN: 1610-1642</identifier><identifier>DOI: 10.1002/pssc.201600107</identifier><language>eng</language><ispartof>Physica status solidi. C, 2016-12, Vol.13 (10-12), p.965-971</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c847-e9e374d4fa705b10724e830980ceffd9e264f4cfaa0fe42275c55b48284c057d3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Sheftel, Elena N.</creatorcontrib><creatorcontrib>Tedzhetov, Valentin A.</creatorcontrib><creatorcontrib>Harin, Eugene V.</creatorcontrib><creatorcontrib>Kiryukhantsev‐Korneev, Filipp V.</creatorcontrib><creatorcontrib>Usmanova, Galina Sh</creatorcontrib><title>High‐induction nanocrystalline soft magnetic Fe X Ti Y B Z films prepared by magnetron sputtering</title><title>Physica status solidi. C</title><description>To design films with the Fe/TiB
2
nanocomposite structure, which are characterized by high saturation induction
B
s
, the phase and structural states and static magnetic properties of Fe‐TiB
2
films prepared by magnetron sputtering and subjected to subsequent annealing have been studied. According to X‐ray diffraction data, either amorphous or nanocrystalline single‐phase structure (an α‐Fe(Ti,B) supersaturated solid solution with a bcc crystal lattice) is formed in the as‐sputtered films. Depending on the film composition, the grain size of the α‐Fe(Ti,B) phase varies from 45.6 to 6.5 nm; grains are characterized by high microstrain (0.21‐4.96%). The annealing at 200‐500 °C leads to a decrease in the lattice parameter of the α‐Fe(Ti,B) phase, i.e. to its depletion of titanium and boron and to the formation of two‐phase α‐Fe + Fe
3
B structure after annealing at 500 °C. The annealing at 200‐500 °C almost does not affect the grain size and microstrain of the bcc α‐Fe‐based phase. The amorphous state of the films is stable up to 500 °C. All studied films are ferromagnets; the saturation induction
B
s
(0.95‐2.13 T) and coercive field
H
c
(0.4‐5 kA/m) of the films were determined. Correlations between the
B
s
and
H
c
magnitudes and the chemical composition of the films, their phase and structural states and magnetic structure are discussed. (© 2016 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)</description><issn>1862-6351</issn><issn>1610-1642</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNo9kL1OwzAUhS0EEqWwMvsFEq4dOz8jVJQiVWLJACyR41wHo8SJ7HTIxiPwjDwJqaiYzhmOPul8hNwyiBkAvxtD0DEHlgIwyM7IiqUMIpYKfr70POVRmkh2Sa5C-ARI5LJcEb2z7cfP17d1zUFPdnDUKTdoP4dJdZ11SMNgJtqr1uFkNd0ifaWlpW_0gb5TY7s-0NHjqDw2tJ5PQ79wwniYJvTWtdfkwqgu4M0p16TcPpabXbR_eXre3O8jnYsswgKTTDTCqAxkvTzgAvMEihw0GtMUyFNhhDZKgUHBeSa1lLXIeS40yKxJ1iT-w2o_hODRVKO3vfJzxaA6GqqOhqp_Q8kvUGVbvg</recordid><startdate>201612</startdate><enddate>201612</enddate><creator>Sheftel, Elena N.</creator><creator>Tedzhetov, Valentin A.</creator><creator>Harin, Eugene V.</creator><creator>Kiryukhantsev‐Korneev, Filipp V.</creator><creator>Usmanova, Galina Sh</creator><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>201612</creationdate><title>High‐induction nanocrystalline soft magnetic Fe X Ti Y B Z films prepared by magnetron sputtering</title><author>Sheftel, Elena N. ; Tedzhetov, Valentin A. ; Harin, Eugene V. ; Kiryukhantsev‐Korneev, Filipp V. ; Usmanova, Galina Sh</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c847-e9e374d4fa705b10724e830980ceffd9e264f4cfaa0fe42275c55b48284c057d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sheftel, Elena N.</creatorcontrib><creatorcontrib>Tedzhetov, Valentin A.</creatorcontrib><creatorcontrib>Harin, Eugene V.</creatorcontrib><creatorcontrib>Kiryukhantsev‐Korneev, Filipp V.</creatorcontrib><creatorcontrib>Usmanova, Galina Sh</creatorcontrib><collection>CrossRef</collection><jtitle>Physica status solidi. C</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sheftel, Elena N.</au><au>Tedzhetov, Valentin A.</au><au>Harin, Eugene V.</au><au>Kiryukhantsev‐Korneev, Filipp V.</au><au>Usmanova, Galina Sh</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>High‐induction nanocrystalline soft magnetic Fe X Ti Y B Z films prepared by magnetron sputtering</atitle><jtitle>Physica status solidi. C</jtitle><date>2016-12</date><risdate>2016</risdate><volume>13</volume><issue>10-12</issue><spage>965</spage><epage>971</epage><pages>965-971</pages><issn>1862-6351</issn><eissn>1610-1642</eissn><abstract>To design films with the Fe/TiB
2
nanocomposite structure, which are characterized by high saturation induction
B
s
, the phase and structural states and static magnetic properties of Fe‐TiB
2
films prepared by magnetron sputtering and subjected to subsequent annealing have been studied. According to X‐ray diffraction data, either amorphous or nanocrystalline single‐phase structure (an α‐Fe(Ti,B) supersaturated solid solution with a bcc crystal lattice) is formed in the as‐sputtered films. Depending on the film composition, the grain size of the α‐Fe(Ti,B) phase varies from 45.6 to 6.5 nm; grains are characterized by high microstrain (0.21‐4.96%). The annealing at 200‐500 °C leads to a decrease in the lattice parameter of the α‐Fe(Ti,B) phase, i.e. to its depletion of titanium and boron and to the formation of two‐phase α‐Fe + Fe
3
B structure after annealing at 500 °C. The annealing at 200‐500 °C almost does not affect the grain size and microstrain of the bcc α‐Fe‐based phase. The amorphous state of the films is stable up to 500 °C. All studied films are ferromagnets; the saturation induction
B
s
(0.95‐2.13 T) and coercive field
H
c
(0.4‐5 kA/m) of the films were determined. Correlations between the
B
s
and
H
c
magnitudes and the chemical composition of the films, their phase and structural states and magnetic structure are discussed. (© 2016 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)</abstract><doi>10.1002/pssc.201600107</doi><tpages>7</tpages></addata></record> |
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| source | Wiley Online Library Journals Frontfile Complete |
| title | High‐induction nanocrystalline soft magnetic Fe X Ti Y B Z films prepared by magnetron sputtering |
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