Quantitative determination of anti-fungal and insecticide amides in adult plants, plantlets and callus from Piper tuberculatum by reverse-phase high-performance liquid chromatography
A rapid, sensitive and reliable reverse‐phase HPLC method was used for the quantitative determination of the anti‐fungal and insecticide amides, dihydropiplartine (1), piplartine (2), Δα,β‐dihydropiperine (3) and pellitorine (4) in plants in natura, in plantlets in vitro and ex vitro, and in callus...
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| Veröffentlicht in: | Phytochemical analysis 2003-09, Vol.14 (5), p.281-284 |
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| creator | Navickiene, H.M.D Bolzani, V. da S Kato, M.J Pereira, A.M.S Bertoni, B.W Franca, S.C Furlan, M |
| description | A rapid, sensitive and reliable reverse‐phase HPLC method was used for the quantitative determination of the anti‐fungal and insecticide amides, dihydropiplartine (1), piplartine (2), Δα,β‐dihydropiperine (3) and pellitorine (4) in plants in natura, in plantlets in vitro and ex vitro, and in callus of Piper tuberculatum. Well‐resolved peaks were obtained with good detection response and linearity in the range of 15.0–3000 µg/mL. The plants in natura contained compounds 1–4, the plantlets ex vitro and in vitro accumulated compounds 1–2 and 1–4, respectively, while only amide 4 was found in callus. Copyright © 2003 John Wiley & Sons, Ltd. |
| doi_str_mv | 10.1002/pca.716 |
| format | Article |
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Well‐resolved peaks were obtained with good detection response and linearity in the range of 15.0–3000 µg/mL. The plants in natura contained compounds 1–4, the plantlets ex vitro and in vitro accumulated compounds 1–2 and 1–4, respectively, while only amide 4 was found in callus. 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Anal</addtitle><description>A rapid, sensitive and reliable reverse‐phase HPLC method was used for the quantitative determination of the anti‐fungal and insecticide amides, dihydropiplartine (1), piplartine (2), Δα,β‐dihydropiperine (3) and pellitorine (4) in plants in natura, in plantlets in vitro and ex vitro, and in callus of Piper tuberculatum. Well‐resolved peaks were obtained with good detection response and linearity in the range of 15.0–3000 µg/mL. The plants in natura contained compounds 1–4, the plantlets ex vitro and in vitro accumulated compounds 1–2 and 1–4, respectively, while only amide 4 was found in callus. Copyright © 2003 John Wiley & Sons, Ltd.</description><subject>amides</subject><subject>Amides - analysis</subject><subject>antifungal agents</subject><subject>Antifungal Agents - analysis</subject><subject>callus</subject><subject>chemical structure</subject><subject>Chromatography, High Pressure Liquid - methods</subject><subject>Culture Techniques</subject><subject>dihydropiperine</subject><subject>dihydropiplartine</subject><subject>ex vitro plantlets</subject><subject>Fatty Acids, Unsaturated - analysis</subject><subject>HPLC</subject><subject>in vitro plantlets</subject><subject>Insecticides - analysis</subject><subject>leaves</subject><subject>mature plants</subject><subject>Molecular Structure</subject><subject>pellitorine</subject><subject>phytochemicals</subject><subject>Piper</subject><subject>Piper - chemistry</subject><subject>Piper - growth & development</subject><subject>Piper tuberculatum</subject><subject>Piperidines - analysis</subject><subject>Piperidones - analysis</subject><subject>piplartine</subject><subject>plant extracts</subject><subject>Plant Extracts - chemistry</subject><subject>Polyunsaturated Alkamides</subject><subject>quantitative analysis</subject><subject>quantitative determination</subject><subject>reversed-phase high performance liquid chromatography</subject><subject>roots</subject><subject>Spectrum Analysis</subject><subject>stems</subject><issn>0958-0344</issn><issn>1099-1565</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2003</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNp1kM9u1DAQhy0EoktBvAH4xgFS7NjObo7VCgrSCpZCxdGaOOONwflT2ynsi_F8uKSCExfP2PPNJ_lHyFPOzjhj5evJwNmaV_fIirO6Lriq1H2yYrXaFExIeUIexfiNsTyrq4fkhEvFVe5X5NenGYbkEiR3g7TFhKF3Q76NAx0tvZ0Vdh4O4HPfUjdENMkZ1yKFPp8xP1FoZ5_o5DMdXy3VY4p_Ngx4P0dqw9jTvZsw0DQ3GMzsIc09bY404A2GiMXUQUTauUNXZMyOoYfBIPXuenbZ02UDpPEQYOqOj8kDCz7ik7t6Sq7evvmyfVfsPl68357vCiMlrwoDKCF_m62VsKYWFkqDrDJWoBRNK4BtDK-l5XVZV41VbSlsKUHazcasWSnEKXmxeE0YYwxo9RRcD-GoOdO3yeucvM7JZ_LZQk5z02P7j7uLOgMvF-CH83j8n0fvt-eLrlhoFxP-_EtD-K6rtVgr_fXDheb15SVnfK93mX--8BZGDYfgor76XDIuGGeiLJUSvwGDDaoa</recordid><startdate>200309</startdate><enddate>200309</enddate><creator>Navickiene, H.M.D</creator><creator>Bolzani, V. da S</creator><creator>Kato, M.J</creator><creator>Pereira, A.M.S</creator><creator>Bertoni, B.W</creator><creator>Franca, S.C</creator><creator>Furlan, M</creator><general>John Wiley & Sons, Ltd</general><scope>FBQ</scope><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>200309</creationdate><title>Quantitative determination of anti-fungal and insecticide amides in adult plants, plantlets and callus from Piper tuberculatum by reverse-phase high-performance liquid chromatography</title><author>Navickiene, H.M.D ; Bolzani, V. da S ; Kato, M.J ; Pereira, A.M.S ; Bertoni, B.W ; Franca, S.C ; Furlan, M</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4416-cae4a0000753fc93fa2ce06cf3e43bd3a08c194f19296bf5d23f24a4f88c70233</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2003</creationdate><topic>amides</topic><topic>Amides - analysis</topic><topic>antifungal agents</topic><topic>Antifungal Agents - analysis</topic><topic>callus</topic><topic>chemical structure</topic><topic>Chromatography, High Pressure Liquid - methods</topic><topic>Culture Techniques</topic><topic>dihydropiperine</topic><topic>dihydropiplartine</topic><topic>ex vitro plantlets</topic><topic>Fatty Acids, Unsaturated - analysis</topic><topic>HPLC</topic><topic>in vitro plantlets</topic><topic>Insecticides - analysis</topic><topic>leaves</topic><topic>mature plants</topic><topic>Molecular Structure</topic><topic>pellitorine</topic><topic>phytochemicals</topic><topic>Piper</topic><topic>Piper - chemistry</topic><topic>Piper - growth & development</topic><topic>Piper tuberculatum</topic><topic>Piperidines - analysis</topic><topic>Piperidones - analysis</topic><topic>piplartine</topic><topic>plant extracts</topic><topic>Plant Extracts - chemistry</topic><topic>Polyunsaturated Alkamides</topic><topic>quantitative analysis</topic><topic>quantitative determination</topic><topic>reversed-phase high performance liquid chromatography</topic><topic>roots</topic><topic>Spectrum Analysis</topic><topic>stems</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Navickiene, H.M.D</creatorcontrib><creatorcontrib>Bolzani, V. da S</creatorcontrib><creatorcontrib>Kato, M.J</creatorcontrib><creatorcontrib>Pereira, A.M.S</creatorcontrib><creatorcontrib>Bertoni, B.W</creatorcontrib><creatorcontrib>Franca, S.C</creatorcontrib><creatorcontrib>Furlan, M</creatorcontrib><collection>AGRIS</collection><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><jtitle>Phytochemical analysis</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Navickiene, H.M.D</au><au>Bolzani, V. da S</au><au>Kato, M.J</au><au>Pereira, A.M.S</au><au>Bertoni, B.W</au><au>Franca, S.C</au><au>Furlan, M</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Quantitative determination of anti-fungal and insecticide amides in adult plants, plantlets and callus from Piper tuberculatum by reverse-phase high-performance liquid chromatography</atitle><jtitle>Phytochemical analysis</jtitle><addtitle>Phytochem. Anal</addtitle><date>2003-09</date><risdate>2003</risdate><volume>14</volume><issue>5</issue><spage>281</spage><epage>284</epage><pages>281-284</pages><issn>0958-0344</issn><eissn>1099-1565</eissn><abstract>A rapid, sensitive and reliable reverse‐phase HPLC method was used for the quantitative determination of the anti‐fungal and insecticide amides, dihydropiplartine (1), piplartine (2), Δα,β‐dihydropiperine (3) and pellitorine (4) in plants in natura, in plantlets in vitro and ex vitro, and in callus of Piper tuberculatum. Well‐resolved peaks were obtained with good detection response and linearity in the range of 15.0–3000 µg/mL. The plants in natura contained compounds 1–4, the plantlets ex vitro and in vitro accumulated compounds 1–2 and 1–4, respectively, while only amide 4 was found in callus. Copyright © 2003 John Wiley & Sons, Ltd.</abstract><cop>Chichester, UK</cop><pub>John Wiley & Sons, Ltd</pub><pmid>14515999</pmid><doi>10.1002/pca.716</doi><tpages>4</tpages></addata></record> |
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| source | MEDLINE; Wiley Online Library Journals Frontfile Complete |
| subjects | amides Amides - analysis antifungal agents Antifungal Agents - analysis callus chemical structure Chromatography, High Pressure Liquid - methods Culture Techniques dihydropiperine dihydropiplartine ex vitro plantlets Fatty Acids, Unsaturated - analysis HPLC in vitro plantlets Insecticides - analysis leaves mature plants Molecular Structure pellitorine phytochemicals Piper Piper - chemistry Piper - growth & development Piper tuberculatum Piperidines - analysis Piperidones - analysis piplartine plant extracts Plant Extracts - chemistry Polyunsaturated Alkamides quantitative analysis quantitative determination reversed-phase high performance liquid chromatography roots Spectrum Analysis stems |
| title | Quantitative determination of anti-fungal and insecticide amides in adult plants, plantlets and callus from Piper tuberculatum by reverse-phase high-performance liquid chromatography |
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