NMR applications for solid‐phase synthesis: Part I. Suppression of residual polymer signals in 1D 1 H NMR spectroscopy of polymer‐supported species
A simple and readily implemented technique for suppression of polymer signals in 1 H 1D NMR spectroscopy of samples from solid‐phase synthetic methods is described. Based on the 2D TOCSY experiment, and combined with routine magic angle spinning, this sequence can be readily adapted from standard pu...
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Veröffentlicht in: | Magnetic resonance in chemistry 2001-05, Vol.39 (5), p.241-248 |
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Format: | Artikel |
Sprache: | eng |
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