Rapid injection NMR: A simple technique for the observation of reactive intermediates
A system has been designed for the NMR observation (at 60 MHz) of unstable intermediates, with half‐lives of 100 ms, at concentration levels above 10−2 M. Rapid mixing can be achieved in less than 40 ms and a series of eight spectra acquired in less than 1.08 s. Low temperature operation is straight...
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| Veröffentlicht in: | Organic Magnetic Resonance 1981-09, Vol.17 (1), p.59-65 |
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| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
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