Modified EPR-DL method for detection of the spinodal decomposition of 2205 duplex stainless steel
The presented work deals with the possibility of electrochemical detection of the spinodal decomposition of duplex stainless steel's ferritic phase using the modified electrochemical potentiodynamic reactivation double loop (EPR‐DL) method. Specimens of FeCr23Ni6Mo3N (2205) steel exposed to the...
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Veröffentlicht in: | Materials and corrosion 2012-07, Vol.63 (7), p.593-597 |
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description | The presented work deals with the possibility of electrochemical detection of the spinodal decomposition of duplex stainless steel's ferritic phase using the modified electrochemical potentiodynamic reactivation double loop (EPR‐DL) method. Specimens of FeCr23Ni6Mo3N (2205) steel exposed to the model low‐temperature annealing at 420 °C for up to 1000 h were used in the experiment. The specimens were evaluated using potentiodynamic curves measurements in chloride solutions and microhardness measurements. Despite hardening the ferritic phase for up to 1 h, a substantial drop of resistance to attack by chlorides was reported only after 1000 h of annealing. The modified EPR‐DL method in 2 M HCl + 0.1 M KSCN solution enables sensitive identification of the spinodal decomposition rate already from early stages. |
doi_str_mv | 10.1002/maco.201106127 |
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Specimens of FeCr23Ni6Mo3N (2205) steel exposed to the model low‐temperature annealing at 420 °C for up to 1000 h were used in the experiment. The specimens were evaluated using potentiodynamic curves measurements in chloride solutions and microhardness measurements. Despite hardening the ferritic phase for up to 1 h, a substantial drop of resistance to attack by chlorides was reported only after 1000 h of annealing. The modified EPR‐DL method in 2 M HCl + 0.1 M KSCN solution enables sensitive identification of the spinodal decomposition rate already from early stages.</description><identifier>ISSN: 0947-5117</identifier><identifier>EISSN: 1521-4176</identifier><identifier>DOI: 10.1002/maco.201106127</identifier><identifier>CODEN: MTCREQ</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>Applied sciences ; Corrosion ; Corrosion environments ; duplex stainless steel ; EPR-DL ; Exact sciences and technology ; Metals. Metallurgy ; microhardness ; spinodal decomposition</subject><ispartof>Materials and corrosion, 2012-07, Vol.63 (7), p.593-597</ispartof><rights>Copyright © 2012 WILEY‐VCH Verlag GmbH & Co. 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Specimens of FeCr23Ni6Mo3N (2205) steel exposed to the model low‐temperature annealing at 420 °C for up to 1000 h were used in the experiment. The specimens were evaluated using potentiodynamic curves measurements in chloride solutions and microhardness measurements. Despite hardening the ferritic phase for up to 1 h, a substantial drop of resistance to attack by chlorides was reported only after 1000 h of annealing. The modified EPR‐DL method in 2 M HCl + 0.1 M KSCN solution enables sensitive identification of the spinodal decomposition rate already from early stages.</description><subject>Applied sciences</subject><subject>Corrosion</subject><subject>Corrosion environments</subject><subject>duplex stainless steel</subject><subject>EPR-DL</subject><subject>Exact sciences and technology</subject><subject>Metals. Metallurgy</subject><subject>microhardness</subject><subject>spinodal decomposition</subject><issn>0947-5117</issn><issn>1521-4176</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqFkEtLAzEURoMoWKtb19m4nJrHJOksa61V6EPExzKkyQ2NTpthMmL7751SLe5c3Qv3O9-Fg9AlJT1KCLteGRt7jFBKJGXqCHWoYDTLqZLHqEOKXGWCUnWKzlJ6J22s4HkHmWl0wQdwePT4lN1O8AqaZXTYxxo7aMA2Ia5x9LhZAk5VWEdnyvZi46qKKfxeGSMCu8-qhA1OjQnrElJqN4DyHJ14Uya4-Jld9HI3eh7eZ5P5-GE4mGSWC6WyheTOWAvOO18wzyAH118UijGhDAhpDVs4Y6QgRDBJKLdOyAXkfcL7TDnKu6i377V1TKkGr6s6rEy91ZTonSC9E6QPglrgag9UJllT-tqsbUgHikkqOWN5myv2ua9QwvafVj0dDOd_f2R7NrQuNgfW1B9aKq6EfpuN9Y2aqeKVc53zb5LOhlg</recordid><startdate>201207</startdate><enddate>201207</enddate><creator>Stoulil, J.</creator><creator>Bystriansky, J.</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><general>Wiley-VCH</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>201207</creationdate><title>Modified EPR-DL method for detection of the spinodal decomposition of 2205 duplex stainless steel</title><author>Stoulil, J. ; Bystriansky, J.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3577-b63daccedfdf92f2e4ed8b972257ae56ca2bdaa6500526013cd56be4803827d13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Applied sciences</topic><topic>Corrosion</topic><topic>Corrosion environments</topic><topic>duplex stainless steel</topic><topic>EPR-DL</topic><topic>Exact sciences and technology</topic><topic>Metals. Metallurgy</topic><topic>microhardness</topic><topic>spinodal decomposition</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Stoulil, J.</creatorcontrib><creatorcontrib>Bystriansky, J.</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Materials and corrosion</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Stoulil, J.</au><au>Bystriansky, J.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Modified EPR-DL method for detection of the spinodal decomposition of 2205 duplex stainless steel</atitle><jtitle>Materials and corrosion</jtitle><addtitle>Materials and Corrosion</addtitle><date>2012-07</date><risdate>2012</risdate><volume>63</volume><issue>7</issue><spage>593</spage><epage>597</epage><pages>593-597</pages><issn>0947-5117</issn><eissn>1521-4176</eissn><coden>MTCREQ</coden><abstract>The presented work deals with the possibility of electrochemical detection of the spinodal decomposition of duplex stainless steel's ferritic phase using the modified electrochemical potentiodynamic reactivation double loop (EPR‐DL) method. Specimens of FeCr23Ni6Mo3N (2205) steel exposed to the model low‐temperature annealing at 420 °C for up to 1000 h were used in the experiment. The specimens were evaluated using potentiodynamic curves measurements in chloride solutions and microhardness measurements. Despite hardening the ferritic phase for up to 1 h, a substantial drop of resistance to attack by chlorides was reported only after 1000 h of annealing. The modified EPR‐DL method in 2 M HCl + 0.1 M KSCN solution enables sensitive identification of the spinodal decomposition rate already from early stages.</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/maco.201106127</doi><tpages>5</tpages></addata></record> |
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subjects | Applied sciences Corrosion Corrosion environments duplex stainless steel EPR-DL Exact sciences and technology Metals. Metallurgy microhardness spinodal decomposition |
title | Modified EPR-DL method for detection of the spinodal decomposition of 2205 duplex stainless steel |
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