Synthesis of deramciclane labeled with tritium in various positions

[(1R)‐endo]‐(+)‐3‐bromocamphor was dehalogenated with tritium gas to [3‐3H]camphor and via [3‐3H]phenylborneol converted to [3‐3H]deramciclane isolated as the fumarate salt (specific activity 51.8 GBq/mmol). This three step synthesis from [3‐3H]camphor gave an overall yield of 22%. Benzyloxy‐acetic...

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Veröffentlicht in:	Journal of labelled compounds & radiopharmaceuticals 2005-08, Vol.48 (9), p.693-700
Hauptverfasser:	Szammer, János, Simon-Trompler, Edit, Banka, Zoltán, Szúnyog, József, Klebovich, Imre
Format:	Artikel
Sprache:	eng
Schlagworte:	4R-(-)-2-(dimethylaminoethoxy)-2-phenyl-1 7-trimethylbicyclo[2.2.1]heptane [2-dimethylamino-[2-3H]ethoxy]deramciclane [3-3H]deramciclane anxiolytic agents 1R anxiolytic agents 1R,2S,4R‐(–)‐2‐(dimethylaminoethoxy)‐2‐phenyl‐1,7,7‐trimethylbicyclo[2.2.1]heptane Biological and medical sciences Contrast media. Radiopharmaceuticals Medical sciences Miscellaneous Pharmacology. Drug treatments tritium
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