Synthesis and characterization of 14 C polyvinylphosphonic acid
Ten mCi of 14 C ethylene was converted to 1.16 mCi of 14 C PVPA by oxidative phosphonation with phosphorus trichloride and molecular oxygen, dehydrohalogenation with triethylamine in ether, polymerization, and hydrolysis. The polymer had a specific activity of 12 uCi/mg and a radiochemical purity ov...
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| Veröffentlicht in: | Journal of labelled compounds & radiopharmaceuticals 1989-06, Vol.27 (6), p.647-652 |
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| Sprache: | eng |
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| container_end_page | 652 |
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| container_issue | 6 |
| container_start_page | 647 |
| container_title | Journal of labelled compounds & radiopharmaceuticals |
| container_volume | 27 |
| creator | Stringer, Orum D. Charig, Andrew |
| description | Ten mCi of
14
C ethylene was converted to 1.16 mCi of
14
C PVPA by oxidative phosphonation with phosphorus trichloride and molecular oxygen, dehydrohalogenation with triethylamine in ether, polymerization, and hydrolysis. The polymer had a specific activity of 12 uCi/mg and a radiochemical purity over 99%. |
| doi_str_mv | 10.1002/jlcr.2580270606 |
| format | Article |
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14
C ethylene was converted to 1.16 mCi of
14
C PVPA by oxidative phosphonation with phosphorus trichloride and molecular oxygen, dehydrohalogenation with triethylamine in ether, polymerization, and hydrolysis. The polymer had a specific activity of 12 uCi/mg and a radiochemical purity over 99%.</description><identifier>ISSN: 0362-4803</identifier><identifier>EISSN: 1099-1344</identifier><identifier>DOI: 10.1002/jlcr.2580270606</identifier><language>eng</language><ispartof>Journal of labelled compounds & radiopharmaceuticals, 1989-06, Vol.27 (6), p.647-652</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-crossref_primary_10_1002_jlcr_25802706063</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Stringer, Orum D.</creatorcontrib><creatorcontrib>Charig, Andrew</creatorcontrib><title>Synthesis and characterization of 14 C polyvinylphosphonic acid</title><title>Journal of labelled compounds & radiopharmaceuticals</title><description>Ten mCi of
14
C ethylene was converted to 1.16 mCi of
14
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14
C ethylene was converted to 1.16 mCi of
14
C PVPA by oxidative phosphonation with phosphorus trichloride and molecular oxygen, dehydrohalogenation with triethylamine in ether, polymerization, and hydrolysis. The polymer had a specific activity of 12 uCi/mg and a radiochemical purity over 99%.</abstract><doi>10.1002/jlcr.2580270606</doi></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0362-4803 |
| ispartof | Journal of labelled compounds & radiopharmaceuticals, 1989-06, Vol.27 (6), p.647-652 |
| issn | 0362-4803 1099-1344 |
| language | eng |
| recordid | cdi_crossref_primary_10_1002_jlcr_2580270606 |
| source | Wiley Online Library Journals Frontfile Complete |
| title | Synthesis and characterization of 14 C polyvinylphosphonic acid |
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