Spherical Zinc Oxide Nano Particles from Zinc Acetate in the Precipitation Method
The liquid precipitation method using zinc acetate dihydrate was applied for the synthesis of uniform and spherical ZnO nanoparticles. The ultrafine zinc oxid was prepared in a water‐ethanol mixture solution. The solution containing zinc cation was soluble in water. The surface‐active agent triethan...
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| Veröffentlicht in: | Journal of the Chinese Chemical Society (Taipei) 2007-02, Vol.54 (1), p.31-34 |
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| container_title | Journal of the Chinese Chemical Society (Taipei) |
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| creator | Hsieh, Cheng-Hsien |
| description | The liquid precipitation method using zinc acetate dihydrate was applied for the synthesis of uniform and spherical ZnO nanoparticles. The ultrafine zinc oxid was prepared in a water‐ethanol mixture solution. The solution containing zinc cation was soluble in water. The surface‐active agent triethanolamine (TEA) was soluble in ethanol. Then alkali precipitated by adding n‐propylamine. The spherical zinc oxide particle morphology was found to be highly dependent on the zinc salt concentration, ethanol‐water ratio, and the surface‐active agent additive. The process can produce white ZnO powder of 50–90 nm in size. The morphology of zinc oxide showed a powder shape by transmission electron microscopy (TEM), the crystallization phase structure of zinc oxide by X‐ray diffraction (XRD), and the zinc oxide remaining by using an organic analysis by infrared spectroscopy (IR). |
| doi_str_mv | 10.1002/jccs.200700006 |
| format | Article |
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The ultrafine zinc oxid was prepared in a water‐ethanol mixture solution. The solution containing zinc cation was soluble in water. The surface‐active agent triethanolamine (TEA) was soluble in ethanol. Then alkali precipitated by adding n‐propylamine. The spherical zinc oxide particle morphology was found to be highly dependent on the zinc salt concentration, ethanol‐water ratio, and the surface‐active agent additive. The process can produce white ZnO powder of 50–90 nm in size. 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The ultrafine zinc oxid was prepared in a water‐ethanol mixture solution. The solution containing zinc cation was soluble in water. The surface‐active agent triethanolamine (TEA) was soluble in ethanol. Then alkali precipitated by adding n‐propylamine. The spherical zinc oxide particle morphology was found to be highly dependent on the zinc salt concentration, ethanol‐water ratio, and the surface‐active agent additive. The process can produce white ZnO powder of 50–90 nm in size. The morphology of zinc oxide showed a powder shape by transmission electron microscopy (TEM), the crystallization phase structure of zinc oxide by X‐ray diffraction (XRD), and the zinc oxide remaining by using an organic analysis by infrared spectroscopy (IR).</description><subject>n-propylamine</subject><subject>Triethanolamine</subject><subject>Zinc acetate dehydrate</subject><subject>Zinc oxide</subject><issn>0009-4536</issn><issn>2192-6549</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2007</creationdate><recordtype>article</recordtype><recordid>eNqFkEFLw0AQhRdRsFavnvcPpM5uspvkWINWpbWRVgQvy2YzoVvbpOwGbP-9KZHizbkMvDff8HiE3DIYMQB-tzbGjzhADN3IMzLgLOWBFFF6TgadlAaRCOUlufJ-DRCFXKQD8rbYrdBZozf009aGzve2RPqq64bm2rXWbNDTyjXb3h4bbHWL1Na0XSHNHRq7s51km5rOsF015TW5qPTG483vHpL3x4dl9hRM55PnbDwNTJiGMmAgiiISuqrKLnwVA6LGuCxACkgRTMIlcCm5jEPBTJlqrJIiAcmSAmOMdTgko_6vcY33Diu1c3ar3UExUMdC1LEQdSqkA9Ie-LYbPPxzrV6ybPGXDXrW-hb3J1a7L9UFjIX6eJ2oJcvzfHafqDz8AV5vdAI</recordid><startdate>200702</startdate><enddate>200702</enddate><creator>Hsieh, Cheng-Hsien</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>200702</creationdate><title>Spherical Zinc Oxide Nano Particles from Zinc Acetate in the Precipitation Method</title><author>Hsieh, Cheng-Hsien</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3936-105bb45affd002f70eeae7db06509e0c8260266267351cd9aef8b80618be7e7a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2007</creationdate><topic>n-propylamine</topic><topic>Triethanolamine</topic><topic>Zinc acetate dehydrate</topic><topic>Zinc oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hsieh, Cheng-Hsien</creatorcontrib><collection>Istex</collection><collection>CrossRef</collection><jtitle>Journal of the Chinese Chemical Society (Taipei)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hsieh, Cheng-Hsien</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Spherical Zinc Oxide Nano Particles from Zinc Acetate in the Precipitation Method</atitle><jtitle>Journal of the Chinese Chemical Society (Taipei)</jtitle><addtitle>Jnl Chinese Chemical Soc</addtitle><date>2007-02</date><risdate>2007</risdate><volume>54</volume><issue>1</issue><spage>31</spage><epage>34</epage><pages>31-34</pages><issn>0009-4536</issn><eissn>2192-6549</eissn><abstract>The liquid precipitation method using zinc acetate dihydrate was applied for the synthesis of uniform and spherical ZnO nanoparticles. The ultrafine zinc oxid was prepared in a water‐ethanol mixture solution. The solution containing zinc cation was soluble in water. The surface‐active agent triethanolamine (TEA) was soluble in ethanol. Then alkali precipitated by adding n‐propylamine. The spherical zinc oxide particle morphology was found to be highly dependent on the zinc salt concentration, ethanol‐water ratio, and the surface‐active agent additive. The process can produce white ZnO powder of 50–90 nm in size. The morphology of zinc oxide showed a powder shape by transmission electron microscopy (TEM), the crystallization phase structure of zinc oxide by X‐ray diffraction (XRD), and the zinc oxide remaining by using an organic analysis by infrared spectroscopy (IR).</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/jccs.200700006</doi><tpages>4</tpages></addata></record> |
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| source | Wiley Online Library All Journals |
| subjects | n-propylamine Triethanolamine Zinc acetate dehydrate Zinc oxide |
| title | Spherical Zinc Oxide Nano Particles from Zinc Acetate in the Precipitation Method |
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