One‐pot Electrochemical Synthesis of Ni Nanoparticles‐decorated Electroreduced Graphene Oxide for Improved NADH Sensing
Ni nanoparticles (NPs) decorated electrochemical reduced graphene oxide (NiNPs/ERGO) nanocomposites (NCs) on ITO electrode were successfully fabricated using one‐pot simultaneously electrochemical co‐reduction method at room temperature. The NiNPs/ERGO electrodes demonstrated very good electrocataly...
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Veröffentlicht in: | Electroanalysis (New York, N.Y.) N.Y.), 2020-10, Vol.32 (10), p.2323-2329 |
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creator | Urhan, Bingül Kurt Öztürk Doğan, Hülya Öznülüer Özer, Tuba Demir, Ümit |
description | Ni nanoparticles (NPs) decorated electrochemical reduced graphene oxide (NiNPs/ERGO) nanocomposites (NCs) on ITO electrode were successfully fabricated using one‐pot simultaneously electrochemical co‐reduction method at room temperature. The NiNPs/ERGO electrodes demonstrated very good electrocatalytic activity in the oxidation of NADH at a low oxidation potential (∼+430 mV), a wide linear range (1–500 μM), a calculated detection limit of 0.002 μM. Compared to ERGO and NiNPs electrodes, the synthesized NiNPs/ERGO NCs have high electrocatalytic activity due to synergistic effect emerged between NiNPs and ERGO. The results indicated that the NiNPs/ERGO NCs can be easily prepared by one‐pot electrochemical technique and NiNPs/ERGO could used to as potential biosensor for the NADH detection. |
doi_str_mv | 10.1002/elan.202060117 |
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The NiNPs/ERGO electrodes demonstrated very good electrocatalytic activity in the oxidation of NADH at a low oxidation potential (∼+430 mV), a wide linear range (1–500 μM), a calculated detection limit of 0.002 μM. Compared to ERGO and NiNPs electrodes, the synthesized NiNPs/ERGO NCs have high electrocatalytic activity due to synergistic effect emerged between NiNPs and ERGO. The results indicated that the NiNPs/ERGO NCs can be easily prepared by one‐pot electrochemical technique and NiNPs/ERGO could used to as potential biosensor for the NADH detection.</description><identifier>ISSN: 1040-0397</identifier><identifier>EISSN: 1521-4109</identifier><identifier>DOI: 10.1002/elan.202060117</identifier><language>eng</language><subject>Electrochemical reduction ; Electrooxidation of NADH ; NADH sensing ; Ni nanoparticles ; reduced graphene oxide</subject><ispartof>Electroanalysis (New York, N.Y.), 2020-10, Vol.32 (10), p.2323-2329</ispartof><rights>2020 Wiley‐VCH GmbH</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3267-91c7bd45b0d1a65425e1fa168da6a052bee7a2f3fba371f4557ac2a94d1a79143</citedby><cites>FETCH-LOGICAL-c3267-91c7bd45b0d1a65425e1fa168da6a052bee7a2f3fba371f4557ac2a94d1a79143</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Felan.202060117$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Felan.202060117$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids></links><search><creatorcontrib>Urhan, Bingül Kurt</creatorcontrib><creatorcontrib>Öztürk Doğan, Hülya</creatorcontrib><creatorcontrib>Öznülüer Özer, Tuba</creatorcontrib><creatorcontrib>Demir, Ümit</creatorcontrib><title>One‐pot Electrochemical Synthesis of Ni Nanoparticles‐decorated Electroreduced Graphene Oxide for Improved NADH Sensing</title><title>Electroanalysis (New York, N.Y.)</title><description>Ni nanoparticles (NPs) decorated electrochemical reduced graphene oxide (NiNPs/ERGO) nanocomposites (NCs) on ITO electrode were successfully fabricated using one‐pot simultaneously electrochemical co‐reduction method at room temperature. The NiNPs/ERGO electrodes demonstrated very good electrocatalytic activity in the oxidation of NADH at a low oxidation potential (∼+430 mV), a wide linear range (1–500 μM), a calculated detection limit of 0.002 μM. Compared to ERGO and NiNPs electrodes, the synthesized NiNPs/ERGO NCs have high electrocatalytic activity due to synergistic effect emerged between NiNPs and ERGO. The results indicated that the NiNPs/ERGO NCs can be easily prepared by one‐pot electrochemical technique and NiNPs/ERGO could used to as potential biosensor for the NADH detection.</description><subject>Electrochemical reduction</subject><subject>Electrooxidation of NADH</subject><subject>NADH sensing</subject><subject>Ni nanoparticles</subject><subject>reduced graphene oxide</subject><issn>1040-0397</issn><issn>1521-4109</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><recordid>eNqFkMtOwzAQRS0EEqWwZe0fSBk7ToyXVSltpSpdFNaR44xpUBpHdnhUbPgEvpEvIVV5LFnNjO49sziEXDIYMQB-hbVuRhw4pMCYPCIDlnAWCQbquN9BQASxkqfkLIRHAFCpUAPytmrw8_2jdR2d1mg678wGt5XRNV3vmm6DoQrUWZpVNNONa7XvKlNj6JkSjfO6w_KH9Fg-mf6ced1usEG6eq1KpNZ5uti23j33WTa-mdM1NqFqHs7JidV1wIvvOST3t9O7yTxarmaLyXgZmZinMlLMyKIUSQEl02kieILMapZelzrVkPACUWpuY1voWDIrkkRqw7USfV0qJuIhGR3-Gu9C8Gjz1ldb7Xc5g3yvLt-ry3_V9YA6AC9Vjbt_2vl0Oc7-2C9MpHcD</recordid><startdate>202010</startdate><enddate>202010</enddate><creator>Urhan, Bingül Kurt</creator><creator>Öztürk Doğan, Hülya</creator><creator>Öznülüer Özer, Tuba</creator><creator>Demir, Ümit</creator><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>202010</creationdate><title>One‐pot Electrochemical Synthesis of Ni Nanoparticles‐decorated Electroreduced Graphene Oxide for Improved NADH Sensing</title><author>Urhan, Bingül Kurt ; Öztürk Doğan, Hülya ; Öznülüer Özer, Tuba ; Demir, Ümit</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3267-91c7bd45b0d1a65425e1fa168da6a052bee7a2f3fba371f4557ac2a94d1a79143</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Electrochemical reduction</topic><topic>Electrooxidation of NADH</topic><topic>NADH sensing</topic><topic>Ni nanoparticles</topic><topic>reduced graphene oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Urhan, Bingül Kurt</creatorcontrib><creatorcontrib>Öztürk Doğan, Hülya</creatorcontrib><creatorcontrib>Öznülüer Özer, Tuba</creatorcontrib><creatorcontrib>Demir, Ümit</creatorcontrib><collection>CrossRef</collection><jtitle>Electroanalysis (New York, N.Y.)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Urhan, Bingül Kurt</au><au>Öztürk Doğan, Hülya</au><au>Öznülüer Özer, Tuba</au><au>Demir, Ümit</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>One‐pot Electrochemical Synthesis of Ni Nanoparticles‐decorated Electroreduced Graphene Oxide for Improved NADH Sensing</atitle><jtitle>Electroanalysis (New York, N.Y.)</jtitle><date>2020-10</date><risdate>2020</risdate><volume>32</volume><issue>10</issue><spage>2323</spage><epage>2329</epage><pages>2323-2329</pages><issn>1040-0397</issn><eissn>1521-4109</eissn><abstract>Ni nanoparticles (NPs) decorated electrochemical reduced graphene oxide (NiNPs/ERGO) nanocomposites (NCs) on ITO electrode were successfully fabricated using one‐pot simultaneously electrochemical co‐reduction method at room temperature. The NiNPs/ERGO electrodes demonstrated very good electrocatalytic activity in the oxidation of NADH at a low oxidation potential (∼+430 mV), a wide linear range (1–500 μM), a calculated detection limit of 0.002 μM. Compared to ERGO and NiNPs electrodes, the synthesized NiNPs/ERGO NCs have high electrocatalytic activity due to synergistic effect emerged between NiNPs and ERGO. The results indicated that the NiNPs/ERGO NCs can be easily prepared by one‐pot electrochemical technique and NiNPs/ERGO could used to as potential biosensor for the NADH detection.</abstract><doi>10.1002/elan.202060117</doi><tpages>7</tpages></addata></record> |
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subjects | Electrochemical reduction Electrooxidation of NADH NADH sensing Ni nanoparticles reduced graphene oxide |
title | One‐pot Electrochemical Synthesis of Ni Nanoparticles‐decorated Electroreduced Graphene Oxide for Improved NADH Sensing |
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