Synthesis of Calixarene-Linked Discotic Triphenylene
The syntheses of new macrocyclic molecules containing calixarene and discotic triphenylene units in good yields are reported. Structural and conformational characterization of these new compounds was achieved by UV/Vis, FTIR, and NMR spectroscopy; mass spectrometry; and elemental analysis. The liqui...
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| Veröffentlicht in: | European Journal of Organic Chemistry 2011-09, Vol.2011 (26), p.5141-5145 |
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| container_issue | 26 |
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| container_title | European Journal of Organic Chemistry |
| container_volume | 2011 |
| creator | Yang, Fafu Guo, Hongyu Xie, Jianwei Lin, Jianrong |
| description | The syntheses of new macrocyclic molecules containing calixarene and discotic triphenylene units in good yields are reported. Structural and conformational characterization of these new compounds was achieved by UV/Vis, FTIR, and NMR spectroscopy; mass spectrometry; and elemental analysis. The liquid‐crystalline behavior was studied by polarizing optical microscopy, differential scanning calorimetry, and X‐ray diffraction. The symmetrical calix[4]arene‐linked triphenylene dimer with a C10 chain (2b) exhibited the liquid‐crystalline behavior of a calixarene bowlic column with two triphenylene units as ancillary lateral columns.
The first calixarene‐linked triphenylenes have been synthesized and their mesomorphic properties studied. The symmetrical calix[4]arene‐linked triphenylene dimer with a C10 chain exhibited the liquid‐crystalline behavior of a calixarene bowlic column with two triphenylene units as ancillary lateral columns. |
| doi_str_mv | 10.1002/ejoc.201100685 |
| format | Article |
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The first calixarene‐linked triphenylenes have been synthesized and their mesomorphic properties studied. The symmetrical calix[4]arene‐linked triphenylene dimer with a C10 chain exhibited the liquid‐crystalline behavior of a calixarene bowlic column with two triphenylene units as ancillary lateral columns.</description><identifier>ISSN: 1434-193X</identifier><identifier>EISSN: 1099-0690</identifier><identifier>DOI: 10.1002/ejoc.201100685</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>Alicyclic compounds ; Alicyclic compounds, terpenoids, prostaglandins, steroids ; Calixarenes ; Chemistry ; Condensed benzenic and aromatic compounds ; Exact sciences and technology ; Mesophases ; Organic chemistry ; Preparations and properties ; Synthesis design ; Triphenylene</subject><ispartof>European Journal of Organic Chemistry, 2011-09, Vol.2011 (26), p.5141-5145</ispartof><rights>Copyright © 2011 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3575-886eb8825f46dda77430e45957ea09df79853a2c1671bfbd87efef90ea5e3b2e3</citedby><cites>FETCH-LOGICAL-c3575-886eb8825f46dda77430e45957ea09df79853a2c1671bfbd87efef90ea5e3b2e3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fejoc.201100685$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fejoc.201100685$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>313,314,780,784,792,1417,27922,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=24519789$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Yang, Fafu</creatorcontrib><creatorcontrib>Guo, Hongyu</creatorcontrib><creatorcontrib>Xie, Jianwei</creatorcontrib><creatorcontrib>Lin, Jianrong</creatorcontrib><title>Synthesis of Calixarene-Linked Discotic Triphenylene</title><title>European Journal of Organic Chemistry</title><addtitle>Eur. J. Org. Chem</addtitle><description>The syntheses of new macrocyclic molecules containing calixarene and discotic triphenylene units in good yields are reported. Structural and conformational characterization of these new compounds was achieved by UV/Vis, FTIR, and NMR spectroscopy; mass spectrometry; and elemental analysis. The liquid‐crystalline behavior was studied by polarizing optical microscopy, differential scanning calorimetry, and X‐ray diffraction. The symmetrical calix[4]arene‐linked triphenylene dimer with a C10 chain (2b) exhibited the liquid‐crystalline behavior of a calixarene bowlic column with two triphenylene units as ancillary lateral columns.
The first calixarene‐linked triphenylenes have been synthesized and their mesomorphic properties studied. The symmetrical calix[4]arene‐linked triphenylene dimer with a C10 chain exhibited the liquid‐crystalline behavior of a calixarene bowlic column with two triphenylene units as ancillary lateral columns.</description><subject>Alicyclic compounds</subject><subject>Alicyclic compounds, terpenoids, prostaglandins, steroids</subject><subject>Calixarenes</subject><subject>Chemistry</subject><subject>Condensed benzenic and aromatic compounds</subject><subject>Exact sciences and technology</subject><subject>Mesophases</subject><subject>Organic chemistry</subject><subject>Preparations and properties</subject><subject>Synthesis design</subject><subject>Triphenylene</subject><issn>1434-193X</issn><issn>1099-0690</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFj71PwzAQxS0EEqWwMmdhTLHj-GtEgRZQRRGUls1ykrPqNiSVXYnmvydVUMXGdHe693tPD6FrgkcE4-QW1k0xSjDpDi7ZCRoQrFSMucKn3Z7SNCaKfp6jixDWGGPFORmg9L2tdysILkSNjTJTub3xUEM8dfUGyujehaLZuSKae7ddQd1W3fMSnVlTBbj6nUP0MX6YZ4_xdDZ5yu6mcUGZYLGUHHIpE2ZTXpZGiJRiSJliAgxWpRVKMmqSgnBBcpuXUoAFqzAYBjRPgA7RqPctfBOCB6u33n0Z32qC9aGzPnTWx84dcNMDWxMKU1lv6sKFI5WkjCghVadTve7bVdD-46ofnmfZ34y4Z13Ywf7IGr_RXFDB9PJloseLyWL5-qb0mP4AtGB3oA</recordid><startdate>201109</startdate><enddate>201109</enddate><creator>Yang, Fafu</creator><creator>Guo, Hongyu</creator><creator>Xie, Jianwei</creator><creator>Lin, Jianrong</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><general>Wiley-VCH</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>201109</creationdate><title>Synthesis of Calixarene-Linked Discotic Triphenylene</title><author>Yang, Fafu ; Guo, Hongyu ; Xie, Jianwei ; Lin, Jianrong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3575-886eb8825f46dda77430e45957ea09df79853a2c1671bfbd87efef90ea5e3b2e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Alicyclic compounds</topic><topic>Alicyclic compounds, terpenoids, prostaglandins, steroids</topic><topic>Calixarenes</topic><topic>Chemistry</topic><topic>Condensed benzenic and aromatic compounds</topic><topic>Exact sciences and technology</topic><topic>Mesophases</topic><topic>Organic chemistry</topic><topic>Preparations and properties</topic><topic>Synthesis design</topic><topic>Triphenylene</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Fafu</creatorcontrib><creatorcontrib>Guo, Hongyu</creatorcontrib><creatorcontrib>Xie, Jianwei</creatorcontrib><creatorcontrib>Lin, Jianrong</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>European Journal of Organic Chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yang, Fafu</au><au>Guo, Hongyu</au><au>Xie, Jianwei</au><au>Lin, Jianrong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Calixarene-Linked Discotic Triphenylene</atitle><jtitle>European Journal of Organic Chemistry</jtitle><addtitle>Eur. J. Org. Chem</addtitle><date>2011-09</date><risdate>2011</risdate><volume>2011</volume><issue>26</issue><spage>5141</spage><epage>5145</epage><pages>5141-5145</pages><issn>1434-193X</issn><eissn>1099-0690</eissn><abstract>The syntheses of new macrocyclic molecules containing calixarene and discotic triphenylene units in good yields are reported. Structural and conformational characterization of these new compounds was achieved by UV/Vis, FTIR, and NMR spectroscopy; mass spectrometry; and elemental analysis. The liquid‐crystalline behavior was studied by polarizing optical microscopy, differential scanning calorimetry, and X‐ray diffraction. The symmetrical calix[4]arene‐linked triphenylene dimer with a C10 chain (2b) exhibited the liquid‐crystalline behavior of a calixarene bowlic column with two triphenylene units as ancillary lateral columns.
The first calixarene‐linked triphenylenes have been synthesized and their mesomorphic properties studied. The symmetrical calix[4]arene‐linked triphenylene dimer with a C10 chain exhibited the liquid‐crystalline behavior of a calixarene bowlic column with two triphenylene units as ancillary lateral columns.</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/ejoc.201100685</doi><tpages>5</tpages></addata></record> |
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| ispartof | European Journal of Organic Chemistry, 2011-09, Vol.2011 (26), p.5141-5145 |
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| language | eng |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Alicyclic compounds Alicyclic compounds, terpenoids, prostaglandins, steroids Calixarenes Chemistry Condensed benzenic and aromatic compounds Exact sciences and technology Mesophases Organic chemistry Preparations and properties Synthesis design Triphenylene |
| title | Synthesis of Calixarene-Linked Discotic Triphenylene |
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