Synthesis of a Metallamacrocyclic Re(CO)3 Complex Using a Tridentate Bridging Ligand
The reaction of [ReBr3(CO)3][NEt4]2 with 3‐hydroxy‐1,2,3‐benzotriazine‐4(3H)‐one in the presence of base gave the ionic rhenium complex [ReBr(C7H4N3O2)(CO)3][NEt4] (2) which was crystallographically characterized. A neutral metallamacrocycle 3 was obtained upon ion of [NEt4]Br from complex 2. This c...
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| Veröffentlicht in: | European journal of inorganic chemistry 2004-03, Vol.2004 (5), p.964-967 |
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| container_issue | 5 |
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| container_title | European journal of inorganic chemistry |
| container_volume | 2004 |
| creator | Brasey, Thomas Buryak, Andrey Scopelliti, Rosario Severin, Kay |
| description | The reaction of [ReBr3(CO)3][NEt4]2 with 3‐hydroxy‐1,2,3‐benzotriazine‐4(3H)‐one in the presence of base gave the ionic rhenium complex [ReBr(C7H4N3O2)(CO)3][NEt4] (2) which was crystallographically characterized. A neutral metallamacrocycle 3 was obtained upon ion of [NEt4]Br from complex 2. This complex cocrystallizes with an unusual C3‐symmetric [Ag(η2‐benzene)3(OH2)][BF4] complex as evidenced by single‐crystal X‐ray diffraction. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004) |
| doi_str_mv | 10.1002/ejic.200300880 |
| format | Article |
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A neutral metallamacrocycle 3 was obtained upon ion of [NEt4]Br from complex 2. This complex cocrystallizes with an unusual C3‐symmetric [Ag(η2‐benzene)3(OH2)][BF4] complex as evidenced by single‐crystal X‐ray diffraction. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)</description><identifier>ISSN: 1434-1948</identifier><identifier>EISSN: 1099-0682</identifier><identifier>DOI: 10.1002/ejic.200300880</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>Host−guest chemistry ; Metallamacrocycles ; Rhenium ; Silver</subject><ispartof>European journal of inorganic chemistry, 2004-03, Vol.2004 (5), p.964-967</ispartof><rights>Copyright © 2004 WILEY‐VCH Verlag GmbH & Co. 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J. Inorg. Chem</addtitle><description>The reaction of [ReBr3(CO)3][NEt4]2 with 3‐hydroxy‐1,2,3‐benzotriazine‐4(3H)‐one in the presence of base gave the ionic rhenium complex [ReBr(C7H4N3O2)(CO)3][NEt4] (2) which was crystallographically characterized. A neutral metallamacrocycle 3 was obtained upon ion of [NEt4]Br from complex 2. This complex cocrystallizes with an unusual C3‐symmetric [Ag(η2‐benzene)3(OH2)][BF4] complex as evidenced by single‐crystal X‐ray diffraction. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)</description><subject>Host−guest chemistry</subject><subject>Metallamacrocycles</subject><subject>Rhenium</subject><subject>Silver</subject><issn>1434-1948</issn><issn>1099-0682</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2004</creationdate><recordtype>article</recordtype><recordid>eNqFkE1PwkAQhhujiYhePfeoh-Jst_vRo1YEDEpUCN422-0UV0sh3SbSf28bDPHmad5MnmcyeT3vksCAAIQ3-GnNIASgAFLCkdcjEMcBcBketzmiUUDiSJ56Z859QodR3vPmb01Zf6Czzt_kvvafsNZFodfaVBvTmMIa_xWvktk19ZPNelvgzl84W65adF7ZDMta1-jftXHVbad2pcvs3DvJdeHw4nf2vcXDcJ6Mg-lsNElup4GhIYPAMOA863IcYUakTHMWy9RwEwKKXBLCM4yZMJgKEFzGIuKYQiZIHmLIGO17g_3d9lnnKszVtrJrXTWKgOo6UV0n6tBJK8R74dsW2PxDq-HjJPnrBnvXuhp3B1dXX4oLKphaPo_U-3h8z5Yg1Av9AQxrc_s</recordid><startdate>200403</startdate><enddate>200403</enddate><creator>Brasey, Thomas</creator><creator>Buryak, Andrey</creator><creator>Scopelliti, Rosario</creator><creator>Severin, Kay</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>200403</creationdate><title>Synthesis of a Metallamacrocyclic Re(CO)3 Complex Using a Tridentate Bridging Ligand</title><author>Brasey, Thomas ; Buryak, Andrey ; Scopelliti, Rosario ; Severin, Kay</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3250-c5066dc32594ed188bf598bc6c20e7f8116de957ceb707689746eb0d71f2e2553</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2004</creationdate><topic>Host−guest chemistry</topic><topic>Metallamacrocycles</topic><topic>Rhenium</topic><topic>Silver</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Brasey, Thomas</creatorcontrib><creatorcontrib>Buryak, Andrey</creatorcontrib><creatorcontrib>Scopelliti, Rosario</creatorcontrib><creatorcontrib>Severin, Kay</creatorcontrib><collection>Istex</collection><collection>CrossRef</collection><jtitle>European journal of inorganic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Brasey, Thomas</au><au>Buryak, Andrey</au><au>Scopelliti, Rosario</au><au>Severin, Kay</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of a Metallamacrocyclic Re(CO)3 Complex Using a Tridentate Bridging Ligand</atitle><jtitle>European journal of inorganic chemistry</jtitle><addtitle>Eur. J. Inorg. Chem</addtitle><date>2004-03</date><risdate>2004</risdate><volume>2004</volume><issue>5</issue><spage>964</spage><epage>967</epage><pages>964-967</pages><issn>1434-1948</issn><eissn>1099-0682</eissn><abstract>The reaction of [ReBr3(CO)3][NEt4]2 with 3‐hydroxy‐1,2,3‐benzotriazine‐4(3H)‐one in the presence of base gave the ionic rhenium complex [ReBr(C7H4N3O2)(CO)3][NEt4] (2) which was crystallographically characterized. A neutral metallamacrocycle 3 was obtained upon ion of [NEt4]Br from complex 2. This complex cocrystallizes with an unusual C3‐symmetric [Ag(η2‐benzene)3(OH2)][BF4] complex as evidenced by single‐crystal X‐ray diffraction. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)</abstract><cop>Weinheim</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/ejic.200300880</doi><tpages>4</tpages></addata></record> |
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| subjects | Host−guest chemistry Metallamacrocycles Rhenium Silver |
| title | Synthesis of a Metallamacrocyclic Re(CO)3 Complex Using a Tridentate Bridging Ligand |
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